Phlorisovalerophenone合成路线 （共 6 条）
反应条件
boron trifluoride diethyl etherate T=100°C; 2 h;
参考文献
Bharate, Sandip B.; Rodge, Atish; Joshi, Rajendra K.; Kaur, Jaspreet; Srinivasan, Shaila; Senthil Kumar; Kulkarni-Almeida, Asha; Balachandran, Sarala; Balakrishnan, Arun; Vishwakarma, Ram A.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 24 p. 6357 - 6361
反应条件
AlCl3, aluminium chloride in nitrobenzene T=50°C; Friedel Crafts acylation; 1 h;
参考文献
Chauthe, Siddheshwar K.; Bharate, Sandip B.; Sabde, Sudeep; Mitra, Debashis; Bhutani, Kamlesh K.; Singh, Inder P.
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 5 p. 2029 - 2036
反应条件
boron trifluoride diethyl etherate T=100°C; 2 h;
参考文献
Chiba; Takakuwa; Tada; Yoshii
Bioscience, biotechnology, and biochemistry, 1992 , vol. 56, # 11 p. 1769 - 1772
反应条件
1: cc. H2SO4 / acetic acid / 240 h / Ambient temperature
2: 23 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C
View Scheme
参考文献
Crombie, Leslie; Jones, Raymond C. F.; Palmer, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 317 - 332
反应条件
1: cc. H2SO4 / acetic acid / 480 h / Ambient temperature
2: 22 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C
View Scheme
参考文献
Crombie, Leslie; Jones, Raymond C. F.; Palmer, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 317 - 332
反应条件
1: POCl3 / ethyl acetate / 0.5 h / 20 °C
2: potassium hydroxide / methanol / 2 h / Heating
View Scheme
参考文献
Bharate, Sandip B.; Bhutani, Kamlesh K.; Khan, Shabana I.; Tekwani, Babu L.; Jacob, Melissa R.; Khan, Ikhlas A.; Singh, Inder Pal
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 1750 - 1760
