in neat (no solvent)
byproducts: Et2Te; inert atmosphere; dropwise addn. of distibane to 1 equiv. ditelluride at0°C; pumping off Et3Sb and Et2Te, repeated fractional distn. (dynamic vac., 80°C);
参考文献
Dickson, Ron S.; Heazle, Kerryn D.
Journal of Organometallic Chemistry, 1995 , vol. 493, # 1-2 p. 189 - 198
in neat (no solvent)
inert atmosphere; dropwise addn. of 1 equiv. Me4Sb2 to Et2Te2 at 0°C, standing for 1 d; filtration, vac. distn. off of volatiles (bath at 25-30°C); contg. 4percent Et2Te2 as impurity;
参考文献
Dickson, Ron S.; Heazle, Kerryn D.
Journal of Organometallic Chemistry, 1995 , vol. 493, # 1-2 p. 189 - 198
