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乙二醇
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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-丙基苯乙酸
合成路线
（共 15 条）
3166-98-1
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
water; sodium hydroxide 4 h; Reflux;
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
Location in patent: Paragraph 0094; 0095 ;
42373-38-6
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
palladium; acetic acid T=60°C; Hydrogenation;
参考文献
Kindler; Metzendorf; Dschi-yin-Kwok
Chemische Berichte, 1943 , vol. 76, p. 308,313
1093190-16-9
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
1.1: potassium carbonate; methanol / 2 h / 20 °C / |Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / |Inert atmosphere 2.2: 0.5 h / 20 °C / |Inert atmosphere 3.1: hydrogen; palladium 10 on activated carbon / ethyl acetate / 15001.5 Torr 4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere 5.1: triethylamine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 6.1: sodium iodide / acetone / 0.25 h / 20 °C 7.1: N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 8.1: sodium hydroxide; water / 4 h / |Reflux View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
275386-60-2
4-(三甲基硅基乙炔基)苄基甲醇
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
1.1: 1H-imidazole / tetrahydrofuran / 15 h / 0 - 20 °C / |Inert atmosphere 2.1: potassium carbonate; methanol / 2 h / 20 °C / |Inert atmosphere 3.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / |Inert atmosphere 3.2: 0.5 h / 20 °C / |Inert atmosphere 4.1: hydrogen; palladium 10 on activated carbon / ethyl acetate / 15001.5 Torr 5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere 6.1: triethylamine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 7.1: sodium iodide / acetone / 0.25 h / 20 °C 8.1: N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 9.1: sodium hydroxide; water / 4 h / |Reflux View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
1093190-17-0
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / |Inert atmosphere 1.2: 0.5 h / 20 °C / |Inert atmosphere 2.1: hydrogen; palladium 10 on activated carbon / ethyl acetate / 15001.5 Torr 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere 4.1: triethylamine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 5.1: sodium iodide / acetone / 0.25 h / 20 °C 6.1: N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 7.1: sodium hydroxide; water / 4 h / |Reflux View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
82657-70-3
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
1: triethylamine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 2: sodium iodide / acetone / 0.25 h / 20 °C 3: N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 4: sodium hydroxide; water / 4 h / |Reflux View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
1360803-33-3
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
1: N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 2: sodium hydroxide; water / 4 h / |Reflux View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
1224716-84-0
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
1: sodium iodide / acetone / 0.25 h / 20 °C 2: N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 3: sodium hydroxide; water / 4 h / |Reflux View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
1360803-31-1
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
1: hydrogen; palladium 10 on activated carbon / ethyl acetate / 15001.5 Torr 2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere 3: triethylamine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 4: sodium iodide / acetone / 0.25 h / 20 °C 5: N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 6: sodium hydroxide; water / 4 h / |Reflux View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
1360803-32-2
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere 2: triethylamine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 3: sodium iodide / acetone / 0.25 h / 20 °C 4: N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 5: sodium hydroxide; water / 4 h / |Reflux View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
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