1,3,5-三[3-(三甲氧基甲硅烷基)丙基]-1,3,5-三嗪-2,4,6(1H,3H,5H)-三酮合成路线 (共 4 条)
反应条件
formic acid; sodium methylate in methanol T=130 - 214°C; P=10 - 760.051 Torr; pH=5.6 - 10; 0.5 - 1.75 h; Product distribution / selectivity;
参考文献
Childress, R. Shawn; McIntyre, James L.
Patent: US2006/235221 A1, 2006 ;
Location in patent: Page/Page column 4-5 ;
反应条件
1: With sodium methylate T=50°C; 2 h; 2: With formic acid T=135 - 210°C; P=10 - 760.051 Torr; 2.16667 h; Product distribution / selectivity;
参考文献
Childress, R. Shawn; McIntyre, James L.
Patent: US2006/235221 A1, 2006 ;
Location in patent: Page/Page column 4 ;
反应条件
formic acid; sodium methylate T=210°C; P=90 - 210 Torr; 1 h; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US2006/276644 A1, 2006 ;
Location in patent: Page/Page column 5 ;
反应条件
T=210°C; P=100 - 300 Torr; 1.65 - 5.65 h; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US7060849 B1, 2006 ;
Location in patent: Page/Page column 8 ;