2-苄基丙烷-1,3-二醇合成路线 （共 23 条）
反应条件
in chloroform
T=20°C; 0.5 h;
参考文献
Mirilashvili, Sima; Chasid-Rubinstein, Naama; Albeck, Amnon
European Journal of Organic Chemistry, 2010 , # 24 p. 4671 - 4686
反应条件
1: With toluene-4-sulfonic acid in dichloromethane
Acetylation;
2: With water
Hydrolysis;
参考文献
Lee, Jeewoo; Park, Shin-Ung; Kim, Ji-Young; Kim, Jin-Kwan; Lee, Jiyoun; Oh, Uhtaek; Marquez, Victor E.; Beheshti, Maryam; Wang, Qiming J.; Modarres, Shayan; Blumberg, Peter M.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 20 p. 2909 - 2914
反应条件
1: 97 percent / butyllithium / tetrahydrofuran / 3 h / -78 - 20 °C
2: 90 percent / DMAP; Et3N / 20 °C
3: 71 percent / TBAF / tetrahydrofuran / 1 h / 20 °C
View Scheme
参考文献
Wiktelius, Daniel; Larsson, Emma K.; Luthman, Kristina
Tetrahedron Asymmetry, 2006 , vol. 17, # 14 p. 2088 - 2100
