五氟化(4-硝基苯基)硫合成路线 （共 27 条）
反应条件
sodium hydroxide in ethanol T=20°C; 1 h;
参考文献
Beier, Petr; Pastyrikova, Tereza
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 411 - 416
反应条件
hydrogenchloride; iron in ethanol; water T=0 - 20°C; 1 h;
参考文献
Wang, Chao; Yu, Yan-Bo; Fan, Shilu; Zhang, Xingang
Organic Letters, 2013 , vol. 15, # 19 p. 5004 - 5007
反应条件
in N,N-dimethyl-formamide T=20°C; 17 h; Inert atmosphere;
参考文献
USTAV ORGANICKE CHEMIE A BIOCHEMIE AKADEMIE VED CESKE REPUBLIKY, v.v.i.; BEIER, Petr
Patent: WO2012/45290 A1, 2012 ;
Location in patent: Page/Page column 15; 16 ;
反应条件
1: alpha,alpha-dimethylbenzyl hydroperoxide; potassium tert-butylate; ammonia / tetrahydrofuran / 0.25 h / -50 °C 2: hydrogen / ethanol / 3 h / 20 °C View Scheme
参考文献
Beier, Petr; Pastyrikova, Tereza
Tetrahedron Letters, 2011 , vol. 52, # 34 p. 4392 - 4394
反应条件
1: N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere 2: bromine; acetic acid / 24 h / 60 °C / Inert atmosphere View Scheme
参考文献
USTAV ORGANICKE CHEMIE A BIOCHEMIE AKADEMIE VED CESKE REPUBLIKY, v.v.i.; BEIER, Petr
Patent: WO2012/45290 A1, 2012 ;
反应条件
1: potassium tert-butylate; 1,1,1-trimethylhydrazinium iodide / dimethyl sulfoxide / 0.08 h / 20 °C
2: hydrogen / ethanol / 2 h / 20 °C
3: hydrogenchloride / water / 1 h / 70 °C
View Scheme
参考文献
Pastyrikova, Tereza; Iakobson, George; Vida, Norbert; Pohl, Radek; Beier, Petr
European Journal of Organic Chemistry, 2012 , # 11 p. 2123 - 2126
反应条件
1: 99 percent / H2 / Raney nickel / ethanol
2: t-BuONO; CuCl2 / acetonitrile
View Scheme
参考文献
Crowley, Patrick J.; Mitchell, Glynn; Salmon, Roger; Worthington, Paul A.
Chimia, 2004 , vol. 58, # 3 p. 138 - 142
