alpha-咔啉N-氧化物合成路线 （共 3 条）
反应条件
trichlorophosphate in N,N-dimethyl-formamide T=20°C; 24 h;
参考文献
Mahmoud, Kazem Ahmed; Krug, Martin; Wersig, Tom; Slynko, Inna; Schaechtele, Christoph; Totzke, Frank; Sippl, Wolfgang; Hilgeroth, Andreas
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 8 p. 1948 - 1951
反应条件
Multi-step reaction with 3 steps 1: toluene / 18 h / |Reflux2: polyphosphoric acid / 3 h / 160 - 175 °C3: dihydrogen peroxide; acetic acid / 6.5 h / |Reflux
参考文献
Mahmoud, Kazem Ahmed; Krug, Martin; Wersig, Tom; Slynko, Inna; Schaechtele, Christoph; Totzke, Frank; Sippl, Wolfgang; Hilgeroth, Andreas Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 8 p. 1948 - 1951
反应条件
Multi-step reaction with 3 steps 1: toluene / 18 h / |Reflux2: polyphosphoric acid / 3 h / 160 - 175 °C3: dihydrogen peroxide; acetic acid / 6.5 h / |Reflux
参考文献
Mahmoud, Kazem Ahmed; Krug, Martin; Wersig, Tom; Slynko, Inna; Schaechtele, Christoph; Totzke, Frank; Sippl, Wolfgang; Hilgeroth, Andreas Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 8 p. 1948 - 1951
