3,4-二氢-4-甲基-1H-2-苯并吡喃合成路线 (共 5 条)
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile T=0°C; 3 h; Inert atmosphere;
参考文献
Zhou, Mei-Yan; Kong, Shan-Shan; Zhang, Ling-Qiong; Zhao, Ming; Duan, Jin-Ao; Ou-Yang, Zhen; Wang, Min
Tetrahedron Letters, 2013 , vol. 54, # 30 p. 3962 - 3964
反应条件
hydrogenchloride T=20°C;
参考文献
Bailey, William F; Mealy, Michael J; Wiberg, Kenneth B
Organic letters, 2002 , vol. 4, # 5 p. 791 - 794
反应条件
lt;Ni(N,N'-bislt;2-(4,5-dihydrooxazol-2-yl)phenylgt;piperdine)gt;lt;BF4gt;; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide T=20°C; electrolysis, Mg anode, carbon fibre cathode;
参考文献
Clinet, Jean Claude; Dunach, Elisabet
Journal of Organometallic Chemistry, 1995 , vol. 503, # 2 p. C48 - C50
反应条件
titanium tetrachloride in dichloromethane T=20°C; Inert atmosphere;
参考文献
Rioz-Martinez, Ana; De Gonzalo; Torres Pazmino, Daniel E.; Fraaije, Marco-W.; Gotor, Vicente
Journal of Organic Chemistry, 2010 , vol. 75, # 6 p. 2073 - 2076
反应条件
1: dichloromethane / 2.5 h / 20 °C / |Inert atmosphere 2: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 3 h / 0 °C / |Inert atmosphere View Scheme
参考文献
Zhou, Mei-Yan; Kong, Shan-Shan; Zhang, Ling-Qiong; Zhao, Ming; Duan, Jin-Ao; Ou-Yang, Zhen; Wang, Min
Tetrahedron Letters, 2013 , vol. 54, # 30 p. 3962 - 3964