N-(4-氯苯)甲酰胺合成路线 （共 104 条）
反应条件
1: potassium carbonate; calcium chloride 2: 200 - 210 °C View Scheme
参考文献
Chattaway; Orton
Journal of the Chemical Society, 1899 , vol. 75, p. 1050
Journal of the Chemical Society, 1901 , vol. 79, p. 277
反应条件
thionyl chloride; sulfuryl dichloride
参考文献
Barreiro, Gabriela; Kim, Joseph T.; Guimaraes, Cristiano R. W.; Bailey, Christopher M.; Domaoal, Robert A.; Wang, Ligong; Anderson, Karen S.; Jorgensen, William L.
Journal of Medicinal Chemistry, 2007 , vol. 50, # 22 p. 5324 - 5329
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Ambient temperature;
参考文献
Rosowsky, Andre; Forsch, Ronald A.; Queener, Sherry F.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 14 p. 2615 - 2620
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in 1,2-dichloro-ethane 0.0333333 h; Molecular sieveInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 14 p. 2172 - 2175
反应条件
di-tert-butyl peroxide in chlorobenzene T=110°C; 48 h; Further byproducts given;
参考文献
Leardini, Rino; Tundo, Antonio; Zanardi, Giuseppe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3164 - 3167
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate in benzene T=5 - 10°C; 1 h; Heating;
参考文献
Sharma, V. K.; Kumar, A.; Agarwal, K. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 11 p. 1153
反应条件
potassium 1.) THF, 5 h, reflux, 2.) toluene/THF, 8 h, reflux; Multistep reaction. Title compound not separated from byproducts;
参考文献
Goehrmann, B.; Niclas, H.-J.
Journal fuer Praktische Chemie (Leipzig), 1990 , vol. 332, # 6 p. 1054 - 1060
反应条件
bis(trichloromethyl) carbonate; sulfur; triethylamine; selenium in dichloromethane 7 h; Heating;
参考文献
Shan; Bian; Su; Liang
Organic Preparations and Procedures International, 2004 , vol. 36, # 3 p. 283 - 286
反应条件
lead(IV) acetate in tetrachloromethane 0.666667 h; Heating;
参考文献
Leardini, Rino; Zanardi, Giuseppe
Synthesis, 1982 , # 3 p. 225 - 227
反应条件
di-tert-butyl peroxide in chlorobenzene T=110°C; 48 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 3164 - 3167
