5,6,7,8-四氢-2-甲基喹啉合成路线 (共 26 条)
反应条件
hydrogen; trifluoroacetic acid; 10percent Pd/C T=20°C; 60 h;
参考文献
Bell, Thomas W.; Khasanov, Alisher B.; Drew, Michael G. B.
Journal of the American Chemical Society, 2002 , vol. 124, # 47 p. 14092 - 14103
反应条件
1: With toluene-4-sulfonic acid in isopropyl alcohol T=160°C; 5 h; Microwave irradiationInert atmosphere; 2: With triethylamine in isopropyl alcohol
参考文献
Rizk, Toni; Bilodeau, Eric J.-F.; Beauchemin, Andre M.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 44 p. 8325 - 8327
反应条件
hydroxylamine hydrochloride in ethanol Heating;
参考文献
Crabb, Trevor A.; Jupp, Philip A.; Turner, Christopher H.
Organic Magnetic Resonance, 1984 , vol. 22, # 7 p. 424 - 427
反应条件
hydrogen; platinum in trifluoroacetic acid Yield given. Title compound not separated from byproducts;
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Monatshefte fuer Chemie, 1984 , vol. 115, p. 1219 - 1228
反应条件
C20H28ClN2OPRu; potassium tert-butylate in tetrahydrofuran; toluene T=135°C; 24 h; Schlenk techniqueInert atmosphereGlovebox;
参考文献
Srimani, Dipankar; Ben-David, Yehoshoa; Milstein, David
Chemical Communications, 2013 , vol. 49, # 59 p. 6632 - 6634
反应条件
trichlorophosphate in 1,2-dichloro-ethane cyclocondensation; 4 h; Heating;
参考文献
Boruah, Romesh C.; Ahmed, Shahadat; Sharma, Utpal; Sandhu, Jagir S.
Journal of Organic Chemistry, 2000 , vol. 65, # 3 p. 922 - 925
反应条件
hydrogen; aluminum oxide; ruthenium in various solvent(s) T=160°C; P=38786.1 Torr; 1.6 h; Product distribution;
参考文献
Okazaki, Hiroshi; Onishi, Kiyotaka; Soeda, Mahito; Ikefuji, Yoshio; Tamura, Ryuji; Mochida, Isao
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 11 p. 3167 - 3174
反应条件
in chloroform T=100°C; 1.5 h;
参考文献
Sugita, Teruyo; Koyama, Junko; Tagahara, Kiyoshi; Suzuta, Yukio
Heterocycles, 1985 , vol. 23, # 11 p. 2789 - 2792
反应条件
hydrogen; nickel T=200°C; P=7600 Torr; or Ru/C, 100 atm, 150 deg C; Equilibrium constant;
参考文献
Pickard; Lochte
Journal of the American Chemical Society, 1947 , vol. 69, p. 14
参考文献
Chelucci, G.; Cossu, S.; Soccolini, F.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1283 - 1286