异硫氰酸基硫代膦酸 O,O-二乙酯合成路线 （共 24 条）
反应条件
4 A molecular sieve; magnesium sulfate; mercury(II) oxide
1.) acetone, reflux, 1 h, 2.) toluene, reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Grapov, A. F.; Zontova, V. N.; Mel'nikov, N. N.
Doklady Chemistry, 1980 , vol. 251, p. 158 - 160
Dokl. Akad. Nauk SSSR Ser. Khim., 1980 , vol. 251, # 4 p. 882 - 884
参考文献
Zimin, M. G.; Kamalov, R. M.; Cherkasov, R. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 3 p. 482 - 487,423 - 427
反应条件
dithiophosphoric acid O,O-diethyl ester
Further byproducts given;
参考文献
Zimin, M. G.; Kamalov, R. M.; Cherkasov, R. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 3 p. 482 - 487,423 - 427
反应条件
in chloroform
1 h; Heating; Further byproducts given;
参考文献
Fedgenhaeuer; Moll
Zeitschrift fur Chemie, 1980 , vol. 20, # 4 p. 141 - 142
反应条件
T=50°C; Further byproducts given;
参考文献
Zimin, M. G.; Kamalov, R. M.; Cherkasov, R. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 3 p. 482 - 487,423 - 427
参考文献
Skowronska, A.; Burski, J.; Krawczyk, E.; Pakulski, M.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 119 - 126
反应条件
(i) <Ph3PCl>Cl, CH2Cl2, (ii) /BRN= 774277/, (iii) (heating); Multistep reaction;
参考文献
Burski,J. et al.
Journal of the Chemical Society, Chemical Communications, 1978 , p. 940 - 941
参考文献
Skowronska, A.; Burski, J.; Krawczyk, E.; Pakulski, M.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 119 - 126
反应条件
in chloroform
1 h; Heating;
参考文献
Fedgenhaeuer; Moll
Zeitschrift fur Chemie, 1980 , vol. 20, # 4 p. 141 - 142
反应条件
mercury(II) oxide
mltistep reaction, various reaction conditions; Product distribution;
参考文献
Grapov, A. F.; Zontova, V. N.; Mel'nikov, N. N.
Doklady Chemistry, 1980 , vol. 251, p. 158 - 160
Dokl. Akad. Nauk SSSR Ser. Khim., 1980 , vol. 251, # 4 p. 882 - 884
