2-氯-n-甲基-n-苯基乙酰胺合成路线 （共 29 条）
反应条件
1: potassium carbonate; potassium iodide / acetonitrile / 8 h / |Reflux 2: trifluoroacetic acid / dichloromethane / 12 h / 20 °C View Scheme
参考文献
Du, Peng; Xu, Lili; Huang, Jiye; Yu, Kunqian; Zhao, Rui; Gao, Bo; Jiang, Hualiang; Zhao, Weili; Zhen, Xuechu; Fu, Wei
Chemical Biology and Drug Design, 2013 , vol. 82, # 3 p. 326 - 335
参考文献
Bischoff; Pessis
Chemische Berichte, 1901 , vol. 34, p. 2125
反应条件
1: AlCl3 / 160 - 170 °C 2: POCl3 View Scheme
参考文献
Benkli, Kadriye; Demirayak, Seref; Gundogdu-Karaburun, Nalan; Kiraz, Nuri; Iscan, Gokalp; Ucucu, Umit
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 1 p. 174 - 179
反应条件
trichlorophosphate 1.) room temp., 6 h, 2.) 1,2-dichloroethane, room temp., 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Croce, Piero Dalla; Rosa, Concetta La; Ritieni, Alberto
Synthesis, 1989 , # 10 p. 783 - 784
反应条件
1: [Me4N][BF4] / N,N-dimethyl-formamide / |Electrolysis 2: potassium hydroxide / water; ethyl acetate / 1 h / 0 °C View Scheme
参考文献
Pasciak, Erick M.; Sengupta, Arkajyoti; Mubarak, Mohammad S.; Raghavachari, Krishnan; Peters, Dennis G.
Electrochimica Acta, 2014 , vol. 127, p. 159 - 166
反应条件
[Me4N][BF4] in N,N-dimethyl-formamide Electrolysis; Reagent/catalyst;
参考文献
Pasciak, Erick M.; Sengupta, Arkajyoti; Mubarak, Mohammad S.; Raghavachari, Krishnan; Peters, Dennis G.
Electrochimica Acta, 2014 , vol. 127, p. 159 - 166
反应条件
barium isothiocyanate; tetramethyl-ammonium; ethylate T=75°C; Rate constant;
参考文献
Journal of Organic Chemistry, , vol. 63, # 19 p. 6476 - 6479
反应条件
[Me4N][BF4] in N,N-dimethyl-formamide Electrolysis; Reagent/catalyst;
参考文献
Pasciak, Erick M.; Sengupta, Arkajyoti; Mubarak, Mohammad S.; Raghavachari, Krishnan; Peters, Dennis G.
Electrochimica Acta, 2014 , vol. 127, p. 159 - 166
反应条件
barium isothiocyanate; tetramethyl-ammonium; ethylate T=75°C; Rate constant;
参考文献
Cacciapaglia, Roberta; Di Stefano, Stefano; Kelderman, Erik; Mandolini, Luigi; Spadola, Francesco
Journal of Organic Chemistry, 1998 , vol. 63, # 19 p. 6476 - 6479
反应条件
ethanol; potassium hydrosulphide
参考文献
Clark; Hams
Biochemical Journal, 1953 , vol. 55, p. 839,842
