2-(4-甲氧基苯基)-1H-苯并咪唑合成路线 (共 67 条)
反应条件
1: in toluene
T=65°C; Inert atmosphere;
2: With iodine in toluene
T=65°C; Inert atmosphere;
参考文献
Osowska, Karolina; Miljanic, Ognjen S.
Journal of the American Chemical Society, 2011 , vol. 133, # 4 p. 724 - 727
反应条件
piperidine in ethanol
Heating;
参考文献
Bogdanowicz-Szwed, Krystyna; Czarny, Agnieszka
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1993 , vol. 335, # 3 p. 279 - 282
反应条件
in acetonitrile
4 h; Heating;
参考文献
Rao, M Hanmantha; Reddy, A Pandu Ranga; Veeranagaiah, V
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 2 p. 88 - 91
反应条件
1: benzene / 20 °C
2: pyridine / 8 h / 120 °C
View Scheme
参考文献
Singh, Girija S.; Singh, Tarjeet; Lakhan, Ram
Arkivoc, 2012 , vol. 2013, # 2 p. 213 - 219
参考文献
Abdel-Latif, Nehad A.; Sabry, Nermien M.; Mohamed, Ashraf M.; Abdulla, Mohamed M.
Monatshefte fur Chemie, 2007 , vol. 138, # 7 p. 715 - 724
反应条件
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 60 °C
2: 2-iodosylbenzoic acid / dimethyl sulfoxide / 3 h / 25 °C
View Scheme
参考文献
Moorthy, Jarugu Narasimha; Neogi, Ishita
Tetrahedron Letters, 2011 , vol. 52, # 30 p. 3868 - 3871
反应条件
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C
2: 2-iodosylbenzoic acid / dimethyl sulfoxide / 3 h / 25 °C
View Scheme
参考文献
Moorthy, Jarugu Narasimha; Neogi, Ishita
Tetrahedron Letters, 2011 , vol. 52, # 30 p. 3868 - 3871
反应条件
1: selenium(IV) oxide / pyridine / 90 - 110 °C / |Schlenk technique
2: Ru(phen)3(Cl)2; oxygen / dimethyl sulfoxide / 36 h / 32 °C / |Irradiation; |Schlenk technique
View Scheme
参考文献
Liu, Jie; Liu, Qiang; Yi, Hong; Qin, Chu; Bai, Ruopeng; Qi, Xiaotian; Lan, Yu; Lei, Aiwen
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 502 - 506
Angew. Chem., 2014 , vol. 126, # 2 p. 512 - 516,5
反应条件
1: 1,4-dioxane; water / 6 h / 20 °C / |Inert atmosphere
2: acetic acid / 5 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Chang, Meng-Yang; Chan, Chieh-Kai; Chen, Yi-Chia
Heterocycles, 2014 , vol. 89, # 5 p. 1229 - 1236
反应条件
hydrogenchloride in methanol
Heating;
参考文献
Orlov, V. D.; Kolos, N. N.; Zolotarev, B. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 3 p. 318 - 323
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 3 p. 390 - 396