2,2'-二硫代二[N-丁基-苯甲酰胺]合成路线 （共 5 条）
反应条件
pyridine; N-methoxyamine hydrochloride in various solvent(s) 3 h; Heating;
参考文献
Sano, Tomohumi; Takagi, Toshiyuki; Gama, Yasuo; Shibuya, Isao; Shimizu, Masao
Synthesis, 2004 , # 10 p. 1585 - 1588
反应条件
in dichloromethane
T=20°C; 0.5 h;
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
参考文献
Siedlecka; Skarzewski
Polish Journal of Chemistry, 2000 , vol. 74, # 10 p. 1369 - 1374
反应条件
1: thionyl chloride / Reflux
2: dichloromethane / 0.5 h / 20 °C
View Scheme
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
反应条件
1: 44 percent / camphorsulfonic acid / CHCl3 / 72 h / 100 °C
2: 98 percent / 3 h / 100 °C
View Scheme
参考文献
Siedlecka; Skarzewski
Polish Journal of Chemistry, 2000 , vol. 74, # 10 p. 1369 - 1374
