N-(4-硝基苯基)氨基甲酸乙酯合成路线 (共 36 条)
参考文献
Ryan; Connolly
Scientific Proceedings of the Royal Dublin Society, 1922 , vol. 17, p. 126 - 129
Chem.Abstr., 1923 , vol. 17, p. 1792
反应条件
1: PCl5
2: air
3: diethyl ether
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参考文献
Swartz
American Chemical Journal, 1897 , vol. 19, p. 316
参考文献
Brewster; Floyd
Trans.Kansas Acad., 1935 , vol. 38, p. 139,141
反应条件
hydrazine in ethanol
Heating;
参考文献
Grammaticakis,P.
Bulletin de la Societe Chimique de France, 1967 , p. 84 - 94
反应条件
1: ammonium formate; 5 palladium on charcoal / tetrahydrofuran; water / 24 h / 50 °C / |Inert atmosphere
2: sulfuric acid; nitric acid / water / 0.5 h / -5 - 0 °C / |Inert atmosphere
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参考文献
Dipharma Francis S.r.l.; Attolino, Emanuele; Rossi, Roberto; Artico, Marco
Patent: EP2730560 A1, 2014 ;
反应条件
5 palladium on charcoal; ammonium formate in tetrahydrofuran; water
T=50°C; 24 h; Inert atmosphere;
参考文献
DIPHARMA FRANCIS S.r.I; ATTOLINO, Emanuele; ROSSI, Roberto; ARTICO, Marco
Patent: US2014/163252 A1, 2014 ;
Location in patent: Paragraph 0036-0037 ;