2-甲基-3-(4’-甲氧基苯甲酰基)吲哚合成路线 （共 12 条）
反应条件
methylmagnesium bromide in diethyl ether T=0 - 20°C; 1.5 h; Reflux;
参考文献
Gong, Tian-Jun; Cheng, Wan-Min; Su, Wei; Xiao, Bin; Fu, Yao
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1859 - 1862
反应条件
carbon monoxide; potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=45°C; P=760 Torr;
参考文献
Arcadi; Cacchi; Carnicelli; Marinelli
Tetrahedron, 1994 , vol. 50, # 2 p. 437 - 452
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=45°C; P=760 Torr;
参考文献
Arcadi; Cacchi; Carnicelli; Marinelli
Tetrahedron, 1994 , vol. 50, # 2 p. 437 - 452
反应条件
1: 87 percent / Et2NH, CuI / PdCl2(PPh3)2 / dimethylformamide / 7 h / 3040 Torr / Ambient temperature 2: 73 percent / K2CO3 / Pd(PPh3)4 / acetonitrile / 45 °C / 760 Torr View Scheme
参考文献
Arcadi; Cacchi; Carnicelli; Marinelli
Tetrahedron, 1994 , vol. 50, # 2 p. 437 - 452
反应条件
sodium hydride; potassium carbonate in toluene Heating;
参考文献
Eissenstat, Michael A.; Weaver, John D.
Tetrahedron Letters, 1995 , vol. 36, # 12 p. 2029 - 2032
反应条件
tetrahydro-1,4-thiazine; sodium hydride; potassium carbonate in toluene Heating;
参考文献
Eissenstat, Michael A.; Weaver, John D.
Tetrahedron Letters, 1995 , vol. 36, # 12 p. 2029 - 2032
反应条件
1: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver hexafluoroantimonate; copper diacetate; silver carbonate / 1,4-dioxane / 24 h / 110 °C / |Inert atmosphere 2: potassium hydroxide / tetrahydrofuran; ethanol / |Reflux 3: methylmagnesium bromide / diethyl ether / 1.5 h / 0 - 20 °C / |Reflux View Scheme
参考文献
Gong, Tian-Jun; Cheng, Wan-Min; Su, Wei; Xiao, Bin; Fu, Yao
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1859 - 1862
反应条件
1: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver hexafluoroantimonate; copper diacetate; silver carbonate / 1,4-dioxane / 1 h / 110 °C / |Schlenk technique; |Inert atmosphere 2: potassium hydroxide / tetrahydrofuran; ethanol / |Reflux 3: methylmagnesium bromide / diethyl ether / 1.5 h / 0 - 20 °C / |Reflux View Scheme
参考文献
Gong, Tian-Jun; Cheng, Wan-Min; Su, Wei; Xiao, Bin; Fu, Yao
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1859 - 1862
反应条件
1: potassium hydroxide / tetrahydrofuran; ethanol / |Reflux 2: methylmagnesium bromide / diethyl ether / 1.5 h / 0 - 20 °C / |Reflux View Scheme
参考文献
Gong, Tian-Jun; Cheng, Wan-Min; Su, Wei; Xiao, Bin; Fu, Yao
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1859 - 1862
反应条件
1: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver hexafluoroantimonate; copper diacetate; silver carbonate / 1,4-dioxane / 12 h / 110 °C / |Schlenk technique; |Inert atmosphere 2: potassium hydroxide / tetrahydrofuran; ethanol / |Reflux 3: methylmagnesium bromide / diethyl ether / 1.5 h / 0 - 20 °C / |Reflux View Scheme
参考文献
Gong, Tian-Jun; Cheng, Wan-Min; Su, Wei; Xiao, Bin; Fu, Yao
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1859 - 1862
