1-甲基-2-苯基苯并咪唑合成路线 （共 38 条）
反应条件
triphenyl phosphite in pyridine
T=220°C; 0.166667 h; microwave irradiation;
参考文献
Lin, Shou-Yuan; Isome, Yuko; Stewart, Ethan; Liu, Ji-Feng; Yohannes, Daniel; Yu, Libing
Tetrahedron Letters, 2006 , vol. 47, # 17 p. 2883 - 2886
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran; hexane; pentane
T=20°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Truong, Thanh; Daugulis, Olafs
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4243 - 4245
反应条件
sodium hydride in toluene; mineral oil
T=180°C; 23 h;
参考文献
Sluiter, Jonas; Christoffers, Jens
Synlett, 2009 , # 1 p. 63 - 66
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene
T=90°C; 6 h; Product distribution; Further Variations:TemperaturesSolventsPressuresreaction times; microwave irradiation;
参考文献
Shieh, Wen-Chung; Dell, Steven; Repic, Oljan
Organic Letters, 2001 , vol. 3, # 26 p. 4279 - 4281
反应条件
trimethylaluminum chloride in toluene
24 h; Heating;
参考文献
Matsushita, Hana; Lee, Sang-Hyeup; Joung, Meyoungju; Clapham, Bruce; Janda, Kim D.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 313 - 316
反应条件
in water
T=120°C; 16 h; Sealed tube;
参考文献
Hikawa, Hidemasa; Imani, Maki; Suzuki, Hideharu; Yokoyama, Yuusaku; Azumaya, Isao
RSC Advances, 2014 , vol. 4, # 8 p. 3768 - 3773
参考文献
Shieh, Wen-Chung; Dell, Steven J.
Patent: US2003/73848 A1, 2003 ;
反应条件
1: 83 percent / POCl3; Et3N / toluene / 18 h / Heating
2: 90 percent / K2CO3; NaOtBu / Pd(PPh3)4 / toluene / 18 h / Heating
View Scheme
参考文献
Brain, Christopher T; Brunton, Shirley A
Tetrahedron Letters, 2002 , vol. 43, # 10 p. 1893 - 1895
反应条件
1: 83 percent / POCl3; Et3N / toluene / 18 h / Heating
2: 90 percent / K2CO3; NaOtBu / Pd(PPh3)4 / toluene / 18 h / Heating
View Scheme
参考文献
Brain, Christopher T; Brunton, Shirley A
Tetrahedron Letters, 2002 , vol. 43, # 10 p. 1893 - 1895
反应条件
in benzene
5 h; Heating;
参考文献
Kolodyazhnaya, S. N.; Divaeva, L. N.; Zheltikova, N. N.; Simonov, A. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 10 p. 1090 - 1094
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 10 p. 1360 - 1364
