4,4-二甲基-2-戊烯合成路线 （共 18 条）
反应条件
T=25°C; P=650 Torr; 0.333333 h;
参考文献
Blanc, Frederic; Coperet, Christophe; Thivolle-Cazat, Jean; Basset, Jean-Marie; Lesage, Anne; Emsley, Lyndon; Sinha, Amritanshu; Schrock, Richard R.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 8 p. 1216 - 1220
反应条件
lithium chloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=70°C; 24 h;
参考文献
Larock, R. C.; Hershberger, S. S.
Tetrahedron Letters, 1981 , vol. 22, # 26 p. 2443 - 2446
反应条件
1: sodium; benzene 2: H2SO4 <100 percent > / bei der Destillation View Scheme
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4195,4558
反应条件
sulfuric acid bei der Destillation;
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4195,4558
反应条件
triphenyl silane; platinum(II) acetylacetonate 0.416667 h; Irradiation;
参考文献
Wang, Fei; Neckers, Douglas C.
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 634 - 636
反应条件
1: toluene / 24 h / 90 °C 2: 30 percent Spectr. / t-BuOK / toluene / 0.33 h / 30 °C 3: 12 percent Chromat. / tetrahydrofuran / 1 h / 0 °C View Scheme
参考文献
Bandmann, Heinz; Bartik, Tamas; Bauckloh, Sylvia; Behler, Ansgar; Brille, Frank; et al.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1990 , vol. 30, # 6 p. 193 - 204
反应条件
1: 30 percent Spectr. / t-BuOK / toluene / 0.33 h / 30 °C 2: 12 percent Chromat. / tetrahydrofuran / 1 h / 0 °C View Scheme
参考文献
Bandmann, Heinz; Bartik, Tamas; Bauckloh, Sylvia; Behler, Ansgar; Brille, Frank; et al.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1990 , vol. 30, # 6 p. 193 - 204
反应条件
in tetrahydrofuran T=0°C; 1 h;
参考文献
Bandmann, Heinz; Bartik, Tamas; Bauckloh, Sylvia; Behler, Ansgar; Brille, Frank; et al.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1990 , vol. 30, # 6 p. 193 - 204
反应条件
T=400°C; bei der thermischen Zersetzung an Glaswolle;
参考文献
Cramer; Miller
Journal of the American Chemical Society, 1940 , vol. 62, p. 1453
Full Text Show Details
Wibaut et al.
Recueil des Travaux Chimiques des Pays-Bas, 1939 , vol. 58, p. 347
Recueil des Travaux Chimiques des Pays-Bas, 1942 , vol. 61, p. 266,267
反应条件
1: HBr 2: alcoholic KOH-solution View Scheme
参考文献
Faworski; Alexejewa
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1920 , vol. 50, p. 561
Chem. Zentralbl., 1923 , vol. 94, # III p. 998
