三氟甲烷磺酸4-甲基-2-(三甲基硅基)苯酯合成路线 （共 25 条）
反应条件
cesium fluoride; dodecacarbonyl tetracobalt in acetonitrile T=60°C; P=7600.51 Torr; 12 h; Title compound not separated from byproducts.;
参考文献
Chatani; Kamitani; Oshita; Fukumoto; Murai
Journal of the American Chemical Society, 2001 , vol. 123, # 50 p. 12686 - 12687
反应条件
caesium carbonate; cesium fluoride in toluene; acetonitrile T=20 - 75°C; Inert atmosphere; Overall yield = 70 percent; Overall yield = 90.8 mg; regioselective reaction;
参考文献
Sha, Feng; Shen, Hui; Wu, Xin-Yan
European Journal of Organic Chemistry, 2013 , # 13 p. 2537 - 2540
反应条件
1: With cesium fluoride in toluene; acetonitrile T=110°C; 48 h; Inert atmosphereSealed vial; 2: With trifluoroacetic acid T=20°C; 0.333333 h;
参考文献
Pirali, Tracey; Zhang, Fengzhi; Miller, Anna H.; Head, Jenna L.; McAusland, Donald; Greaney, Michael F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 4 p. 1006 - 1009
反应条件
cesium fluoride in tetrahydrofuran T=90°C; 24 h; Title compound not separated from byproducts;
参考文献
Zhao, Jian; Larock, Richard C.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 583 - 588
反应条件
iodine; cesium fluoride in acetonitrile T=20°C; 16 h; Inert atmosphere;
参考文献
Rodriguez-Lojo, Diego; Cobas, Agustin; Pena, Diego; Perez, Dolores; Guitian, Enrique
Organic Letters, 2012 , vol. 14, # 6 p. 1363 - 1365
反应条件
cesium fluoride in acetonitrile
T=20°C; Overall yield = 44 percent;
参考文献
Chakrabarty, Shyamal; Chatterjee, Indranil; Tebben, Ludger; Studer, Armido
Angewandte Chemie - International Edition, 2013 , vol. 52, # 10 p. 2968 - 2971
Angew. Chem., 2013 , vol. 125, # 10 p. 3041 - 3044
反应条件
cesium fluoride in tetrahydrofuran
T=90°C; 24 h; Title compound not separated from byproducts;
参考文献
Zhao, Jian; Larock, Richard C.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 583 - 588
反应条件
cesium fluoride in acetonitrile
T=20°C; 24 h; Further byproducts. Title compound not separated from byproducts.;
参考文献
Beltran-Rodil, Sandra; Pena, Diego; Guitian, Enrique
Synlett, 2007 , # 8 p. 1308 - 1310
反应条件
cesium fluoride
Title compound not separated from byproducts.;
参考文献
Beltran-Rodil, Sandra; Pena, Diego; Guitian, Enrique
Synlett, 2007 , # 8 p. 1308 - 1310
反应条件
cesium fluoride; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) in toluene; acetonitrile
T=110°C; 12 h;
参考文献
Zhang, Xiaoxia; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 18 p. 3973 - 3976
