三氟甲烷磺酸4-甲基-2-(三甲基硅基)苯酯合成路线 (共 25 条)
反应条件
cesium fluoride; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) in toluene; acetonitrile
T=110°C; 12 h;
参考文献
Zhang, Xiaoxia; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 18 p. 3973 - 3976
反应条件
cesium fluoride in tetrahydrofuran
T=90°C; 24 h; Title compound not separated from byproducts;
参考文献
Zhao, Jian; Larock, Richard C.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 583 - 588
反应条件
potassium fluoride; 18-crown-6 ether in tetrahydrofuran
T=0°C; 45.5 h; Title compound not separated from byproducts.;
参考文献
Yoshida, Hiroto; Mimura, Yasuhiro; Ohshita, Joji; Kunai, Atsutaka
Chemical Communications, 2007 , # 23 p. 2405 - 2407
反应条件
cesium fluoride in acetonitrile
T=20°C; Overall yield = 44 percent;
参考文献
Chakrabarty, Shyamal; Chatterjee, Indranil; Tebben, Ludger; Studer, Armido
Angewandte Chemie - International Edition, 2013 , vol. 52, # 10 p. 2968 - 2971
Angew. Chem., 2013 , vol. 125, # 10 p. 3041 - 3044
反应条件
cesium fluoride in tetrahydrofuran
T=90°C; 24 h; Title compound not separated from byproducts;
参考文献
Zhao, Jian; Larock, Richard C.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 583 - 588