2,5,8,11-四氧杂十三碳-12-烯合成路线 (共 4 条)
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; sodium carbonate in toluene T=100°C; 3 h; Inert atmosphere;
参考文献
Harada, Nari-Aki; Nishikata, Takashi; Nagashima, Hideo
Tetrahedron, 2012 , vol. 68, # 15 p. 3243 - 3252
反应条件
1,10-phenanthroline; palladium diacetate in dichloromethane T=60°C; Schlenk techniqueInert atmosphereAutoclave;
参考文献
Alaaeddine, Ali; Hess, Andrew; Boschet, Frederic; Allcock, Harry; Ameduri, Bruno
Journal of Polymer Science, Part A: Polymer Chemistry, 2013 , vol. 51, # 4 p. 977 - 986
反应条件
potassium hydroxide; dimethyl sulfoxide T=76 - 84°C; Etherification; 7.5 h;
参考文献
Parshina; Sokolyanskaya; Nosyreva; Scotheim; Zefirov; Trofimov
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 2 p. 202 - 206
反应条件
1: vinyl methyl ether of triethylene glycol; bis(15-crown-5)potassium potasside
2: benzyl bromide
参考文献
Grobelny, Zbigniew; Stolarzewicz, Andrzej; Maercker, Adalbert; Krompiec, Stanis; Kasperczyk, Janusz; Rzepa, Jozef
Journal of Organometallic Chemistry, 2004 , vol. 689, # 9 p. 1580 - 1585