hydrogenchloride in tetrahydrofuran 20 h; Ambient temperature;
参考文献
Hanson, Peter; Loevenich, P. Wilfried; Rowell, Simon C.; Walton, Paul H.; Timms, Allan W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1999 , # 1 p. 49 - 64
lithium aluminium tetrahydride; tert-butyl alcohol in diethylene glycol dimethyl ether T=-78 - 20°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Braese, Stefan; Ruemper, Joerg; Voigt, Katharia; Albecq, Stephane; Thurau, Gert; et al.
European Journal of Organic Chemistry, 1998 , # 4 p. 671 - 678