(S)-(-)- α-甲基苄胺合成路线 （共 369 条）
参考文献
Crane; Corey
Organic letters, 2001 , vol. 3, # 9 p. 1395 - 1397
反应条件
potassium hydroxide in diethylene glycol T=210°C; 2.5 h;
参考文献
Rahman, S. M. Abdur; Ohno, Hiroaki; Tanaka, Tetsuaki
Tetrahedron Letters, 2001 , vol. 42, # 45 p. 8007 - 8010
反应条件
pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. phosphate buffer T=37°C; pH=7.4; 0.0833333 h; Enzymatic reaction;
参考文献
Jiang, Jinju; Chen, Xi; Feng, Jinhui; Wu, Qiaqing; Zhu, Dunming
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 100, p. 32 - 39
反应条件
lithium perchlorate in acetonitrile 18 h; Heating;
参考文献
Tetrahedron Letters, , vol. 47, # 32 p. 5717 - 5721
反应条件
benzil T=149.85°C; 0.5 h;
参考文献
Vazquez Garcia, Rosa A.; Bernes, Sylvain; Gutierrez Perez, Rene; Martinez Garcia, Marcos
Acta Crystallographica Section C: Crystal Structure Communications, 2002 , vol. 58, # 10 p. o619-o620
反应条件
water; acetic acid; sodium nitrite 1.) RT, 18 h, 2.) 1 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 8, # 13 p. 2193 - 2198
反应条件
1: With Yb(OAc)3 in tetrahydrofuran; methanol T=50°C; 4 h; 2: With hydrogen; platinum on activated charcoal in tetrahydrofuran; methanol T=50°C; P=6205.94 Torr; 20 h;
参考文献
JACOBS UNIVERSITY BREMEN GGMBH
Patent: WO2007/104359 A1, 2007 ;
Location in patent: Page/Page column 25-26 ;
反应条件
hydrogenchloride; hydrogen; Rh/Al2O3 in water T=20°C; Hydrogenation; P=750.06 Torr;
参考文献
Strotmann; Butenschon
Synthetic Communications, 2000 , vol. 30, # 22 p. 4173 - 4176
反应条件
1: With Yb(OAc)3 in tetrahydrofuran; methanol T=20°C; 2 h; 2: With hydrogen; nickel in tetrahydrofuran; methanol T=20°C; P=6205.94 Torr; 24 h;
参考文献
JACOBS UNIVERSITY BREMEN GGMBH
Patent: WO2007/104359 A1, 2007 ;
Location in patent: Page/Page column 25 ;
反应条件
1: With Yb(OAc)3 in tetrahydrofuran; methanol T=20°C; 2 h; 2: With hydrogen; nickel in tetrahydrofuran; methanol P=6225.62 Torr; 18 h; Product distribution / selectivity;
参考文献
JACOBS UNIVERSITY BREMEN GGMBH
Patent: WO2007/104357 A1, 2007 ;
Location in patent: Page/Page column 33 ;
