(S)-(-)- α-甲基苄胺合成路线 （共 369 条）
反应条件
di-tert-butyl peroxide; [IndBox]Cu T=80°C; 24 h;
参考文献
Georgetown University
Patent: US2011/213146 A1, 2011 ;
Location in patent: Page/Page column 3; 27 ;
反应条件
1: p-toluenesulfonic acid / toluene / Heating 2: H2 / Pd/C / tetrahydrofuran / 760 Torr View Scheme
参考文献
Uccello-Barretta; Bernardini; Balzano; Salvadori
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 123 - 129
反应条件
1: sec-phenethyl alcohol With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene in dichloromethane T=20°C; 16 h; 2: (S)-1-phenyl-ethylamine With sodium tris(acetoxy)borohydride in dichloromethane optical yield given as percent dechemoselective reaction;
参考文献
Guerin, Claire; Bellosta, Veronique; Guillamot, Gerard; Cossy, Janine
Organic Letters, 2011 , vol. 13, # 13 p. 3534 - 3537
反应条件
1: titanium(IV) isopropylate / isopropanol acetate / 0.5 h / Inert atmosphere 2: hydrogen / isopropanol acetate / 24 h / 35 °C / 15001.5 Torr View Scheme
参考文献
Nugent, Thomas C.; Negru, Daniela E.; El-Shazly, Mohamed; Hu, Dan; Sadiq, Abdul; Bibi, Ahtaram; Umar, M. Naveed
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2085 - 2092
反应条件
1: titanium(IV) isopropylate / ethyl acetate / 0.5 h / 20 °C 2: hydrogen / ethyl acetate; ethanol / 8 h / 24 °C / 6225.62 Torr View Scheme
参考文献
Nugent, Thomas C.; Marinova, Sofiya M.
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-Z0768-FA, p. 153 - 166
反应条件
hydrogen Yield given;
参考文献
Eleveld, M. B.; Hogeveen, H.
Tetrahedron Letters, 1984 , vol. 25, # 45 p. 5187 - 5190
反应条件
pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. phosphate buffer T=37°C; pH=7.4; 12 h; Enzymatic reaction; Time; enantioselective reaction;
参考文献
Jiang, Jinju; Chen, Xi; Feng, Jinhui; Wu, Qiaqing; Zhu, Dunming
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 100, p. 32 - 39
参考文献
Juaristi, Eusebio; Hernandez-Rodriguez, Marcos; Lopez-Ruiz, Heraclio; Avina, Judit; Munoz-Muniz, Omar; Hayakawa, Michiya; Seebach, Dieter
Helvetica Chimica Acta, 2002 , vol. 85, # 7 p. 1999 - 2008
参考文献
Mastranzo, Virginia M.; Quintero, Leticia; De Parrodi, Cecilia Anaya; Juaristi, Eusebio; Walsh, Patrick J.
Tetrahedron, 2004 , vol. 60, # 8 p. 1781 - 1789
参考文献
Fiorentino, Antonio; DellaGreca, Marina; D'Abrosca, Brigida; Golino, Annunziata; Pacifico, Severina; Izzo, Angelina; Monaco, Pietro
Tetrahedron, 2006 , vol. 62, # 38 p. 8952 - 8958
