反应条件
in neat (no solvent)
(Ar); reaction of Pd complex with excess of C8H18Si2O for 2 h, filtration, cooling (-78°C), crystn.; removal of mother liquor, washing (cold C5H12), drying (in vacuo, 20°C); elem. anal.;
参考文献
Krause, Jochen; Cestaric, Guenter; Haack, Karl-Josef; Seevogel, Klaus; Storm, Werner; Poerschke, Klaus-Richard
Journal of the American Chemical Society, 1999 , vol. 121, # 42 p. 9807 - 9823