6-O-对甲基苯磺酰基-1,2-O-异丙叉-Alpha-D-葡萄糖合成路线 (共 4 条)
反应条件
sodium azide in N,N-dimethyl-formamide T=40°C; 15 h;
参考文献
Fernandez, Jose M. Garcia; Mellet, Carmen Ortiz; Maciejewski, Sylwester; Defaye, Jacques
Journal of the Chemical Society, Chemical Communications, 1996 , # 24 p. 2741 - 2742
参考文献
Vargha et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 261
反应条件
1: 92 percent / NaN3 / dimethylformamide / 20 h / 120 °C
2: 82 percent / aq. TFA / 0.5 h / 40 °C
View Scheme
参考文献
Fernandez, Jose M. Garcia; Mellet, Carmen Ortiz; Maciejewski, Sylwester; Defaye, Jacques
Journal of the Chemical Society, Chemical Communications, 1996 , # 24 p. 2741 - 2742
反应条件
acetic acid
Behandeln mit Acetanhydrid und Pyridin;
参考文献
Ohle; v. Vargha
Chemische Berichte, 1929 , vol. 62, p. 2425,2433
Chemische Berichte, 1928 , vol. 61, p. 1208,1210
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Compton
Journal of the American Chemical Society, 1938 , vol. 60, p. 395,398