反应条件
air in tetrahydrofuran; ammonia
N2-atmosphere; treatment op Ph2SbCl with 2 equiv. of Na (in liquid NH3, -33°C), dropwise addn. to stoich. amt. of ClCH2CH2Cl (in THF), stirring for 4 h, evapn. of NH3, treatment with water and CH2Cl2; sepn. of org. layer, drying, evapn., recrystn. (EtOH/CH2Cl2); elem. anal.;
参考文献
Kian-Kong Chow; Levason, William; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 1429 - 1432
