D-甘露糖酸-1,4-内酯合成路线 (共 22 条)
反应条件
platinum(IV) oxide; water P=1471.02 - 2206.5 Torr; Hydrogenation;
参考文献
Isbell; Karabinos
Journal of Research of the National Bureau of Standards (United States), 1952 , vol. 48, p. 438,439
Org.Synth.Isotopes, 1958 , p. 1046
反应条件
1: 71 percent / CBr4, Ph3P / 2 h / Ambient temperature 2: 58 percent / HClO4 / 2 h 3: 1.) NaBH4, ion exchange resin (IR-120, H+), 2.) AcCl / 1.) EtOH, 2.) EtOH, 5 deg C, overnight View Scheme
参考文献
Lundt, Inge; Frank, Holger
Tetrahedron, 1994 , vol. 50, # 46 p. 13285 - 13298