in acetone; benzene N2-atmosphere; excess of Co-complex, dissoln. in benzene/acetone=1:1 (50°C), stirring (1 h); crystn. on partial evapn., filtration, evapn. of filtrate to dryness;
参考文献
Sacco, A.; Vasapollo, G.; Giannoccaro, P.
Inorganica Chimica Acta, 1979 , vol. 32, p. 171 - 174
in chlorobenzene
stirring under N2 at 40°C for 24 h (TLC monitoring); filtration, washing with MeCN, then with hexane; dissoln. in CH2Cl2, filtration, evapn.; elem. anal.;
参考文献
Baysdon, Sherrol L.; Liebeskind, Lanny S.
Organometallics, 1982 , vol. 1, p. 771 - 775
