1,3,5-三氯-2,4,6-硝基苯合成路线 （共 22 条）
参考文献
Turek
Patent: DE498050 , 1927 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 655
参考文献
Turek
Patent: DE498050 , 1927 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 655
反应条件
ammonia in toluene 10 h; Heating;
参考文献
Kohne, Bernd; Praefcke, Klaus
Liebigs Annalen der Chemie, 1985 , # 3 p. 522 - 528
参考文献
Backer; van der Baan
Recueil des Travaux Chimiques des Pays-Bas, 1937 , vol. 56, p. 1161,1165
Full Text Show Details
Sorm; Drapalova
Chem. Obzor, 1937 , vol. 12, p. 153
Chem. Zentralbl., 1937 , vol. 108, # II p. 4033
反应条件
1: ammonia / toluene / Heating
2: methanol; ammonia; sodium / Cooling
3: ethanol; water / Cooling
View Scheme
参考文献
Juarez, Rafael; Ramos, Mar; Segura, Jose L.; Orduna, Jesus; Villacampa, Belen; Alicante, Raquel
Journal of Organic Chemistry, 2010 , vol. 75, # 22 p. 7542 - 7549
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US5081255 A1, 1992 ;
参考文献
Jackson; Smith
American Chemical Journal, 1904 , vol. 32, p. 173
反应条件
1: 99 percent / NH3-gas / toluene / 10 h / Heating
2: 68 percent / Ph-NH-NH2 / 1.) 120 degC, 2.5 h; 2.) to 140 degC in 2.5 h; 3.) 140 degC, 1h
View Scheme
参考文献
Tao, Zhi-Gang; Zhao, Xin; Jiang, Xi-Kui; Li, Zhan-Ting
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1840 - 1842
反应条件
hydrazine in methanol
参考文献
Lawrence, G. William; Adolph, Horst G.
Tetrahedron Letters, 1980 , vol. 21, p. 1615 - 1618
反应条件
hydrazine
Mechanism;
参考文献
Rees, Charles W.; Smith, David I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1159 - 1164
