alpha-溴-4-甲氧基苯乙酮合成路线 （共 261 条）
反应条件
N-bromosuccinmide; silica gel in methanol 0.216667 h; Reflux; chemoselective reaction;
参考文献
Mohan Reddy, Bodireddy; Venkata Ramana Kumar, Velpula; Chinna Gangi Reddy, Nallagondu; Mahender Rao, Siripragada
Chinese Chemical Letters, 2014 , vol. 25, # 1 p. 179 - 182
反应条件
water; silver fluoride; trifluoroacetic acid T=40°C; 6 h; Green chemistry;
参考文献
Chen, Zheng-Wang; Ye, Dong-Nai; Ye, Min; Zhou, Zhong-Gao; Li, Shen-Huan; Liu, Liang-Xian
Tetrahedron Letters, 2014 , vol. 55, # 7 p. 1373 - 1375
反应条件
bromine in 1,4-dioxane; diethyl ether 0.5 h; Ambient temperature;
参考文献
Rival; Taudou; Ecalle
Farmaco, 1993 , vol. 48, # 6 p. 857 - 869
反应条件
oxygen; sodium nitrite in dichloromethane; water T=25°C; P=760.051 Torr; 6 h; Sealed system;
参考文献
Zhang, Guofu; Wen, Xin; Wang, Yong; Mo, Weimin; Ding, Chengrong
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4665 - 4668
反应条件
phenyltrimethylammonium tribromide in tetrahydrofuran T=25°C; 2.15 h;
参考文献
Cristau, Henri-Jean; Torreilles, Eliane; Morand, Philippe; Christol, Henri
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 25, p. 357 - 368
反应条件
[Ru(II)(2,2’-bipyridine)3]Cl2; DNP; ascorbic acid powder in methanol; water 2 h; Inert atmosphereIrradiation;
参考文献
Maji, Tapan; Karmakar, Ananta; Reiser, Oliver
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 736 - 739
反应条件
dipotassium peroxodisulfate; potassium bromide in water T=60°C; 12 h; Green chemistry;
参考文献
Jiang, Qing; Sheng, Wenbing; Guo, Cancheng
Green Chemistry, 2013 , vol. 15, # 8 p. 2175 - 2179
反应条件
tribromure de triphenylmethylphosphonium in dichloromethane T=25°C; 3 h;
参考文献
Cristau, Henri-Jean; Torreilles, Eliane; Morand, Philippe; Christol, Henri
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 25, p. 357 - 368
反应条件
1: With water T=100°C; 3 h; 2: With dihydrogen peroxide in 1,4-dioxane; water T=25°C; 3 h;
参考文献
Patil, Rajendra D.; Adimurthy, Subbarayappa; Ranu, Brindaban C.
Synthetic Communications, 2010 , vol. 40, # 21 p. 3233 - 3239
反应条件
1: diethyl ether / Umsetzen der entstandenen Magnesiumverbindung mit Bromcyan 2: sulfuric acid View Scheme
参考文献
Xie, Longyong; Wu, Yundong; Yi, Weiguo; Zhu, Lei; Xiang, Jiannan; He, Weimin
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 9190 - 9195
