alpha-溴-4-甲氧基苯乙酮合成路线 （共 261 条）
参考文献
Novartis AG
Patent: US6140332 A1, 2000 ;
US 6140332 A
反应条件
potassium carbonate in ethanol Heating;
参考文献
Pittala, Valeria; Romeo, Giuseppe; Salerno, Loredana; Siracusa, Maria Angela; Modica, Maria; Materia, Luisa; Mereghetti, Ilario; Cagnotto, Alfredo; Mennini, Tiziana; Marucci, Gabriella; Angeli, Piero; Russo, Filippo
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 1 p. 150 - 153
反应条件
sodium ethanolate in ethanol
参考文献
Kaspersen, Svein Jacob; Hoff, Bard Helge; Sundby, Eirik; Charnock, Colin
Bioorganic Chemistry, 2012 , vol. 44, p. 35 - 41,7
反应条件
1.1: sodium ethanolate / ethanol / 0.33 h / 0 °C / Inert atmosphere 1.2: 1.5 h / 60 °C 2.1: formic acid / N,N-dimethyl-formamide / 20 h / 150 °C 3.1: trichlorophosphate / 3 h / 90 °C 3.2: pH 12 View Scheme
参考文献
Kaspersen, Svein Jacob; Hoff, Bard Helge; Sundby, Eirik; Charnock, Colin
Bioorganic Chemistry, 2012 , vol. 44, p. 35 - 41,7
反应条件
1: in ethyl acetate 2: With dihydrogen peroxide T=20°C; 72 h;
参考文献
Kovalenko; Cherepakha; Kutrov; Shishkin; Shishkina
Chemistry of Heterocyclic Compounds, 2012 , vol. 47, # 10 p. 1280 - 1285
反应条件
sodium hydrogencarbonate in ethanol 6 h;
参考文献
Gudmundsson, Kristjan S.; Johns, Brian A.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 10 p. 2735 - 2739
反应条件
water; sodium chloride T=75°C; 0.833333 h; microwave irradiation;
参考文献
Utsukihara, Takamitsu; Nakamura, Hiroaki; Watanabe, Masashige; Akira Horiuchi
Tetrahedron Letters, 2006 , vol. 47, # 52 p. 9359 - 9364
反应条件
1,3-dibenzyl-1H-benzo[d]imidazol-3-ium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=20°C; 0.366667 h; Inert atmosphere;
参考文献
Singh, Santosh; Singh, Pankaj; Rai, Vijai K.; Kapoor, Ritu; Yadav, Lal Dhar S.
Tetrahedron Letters, 2011 , vol. 52, # 1 p. 125 - 128
反应条件
boron trifluoride; silver carbonate T=15°C; 20 h;
参考文献
Giordano, Claudio; Castaldi, Graziano; Casagrande, Francesco; Abis, Luigi
Tetrahedron Letters, 1982 , vol. 23, # 13 p. 1385 - 1386
反应条件
1: p-TsOH / methanol / 1 h 2: AgBF4 / methanol / 25 °C / reaction order and rate constants for the reaction between methyl acetals of primary α-halogenoakyl aryl ketones and AgBF4; reaction with AgNO3; effect of the substituent in aromatic ring View Scheme
参考文献
Giordano, Claudio; Castaldi, Graziano; Casagrande, Francesco; Belli, Aldo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 11 p. 2575 - 2582
