alpha-溴-4-甲氧基苯乙酮合成路线 （共 261 条）
反应条件
1: ethanol / |Reflux 2: sodium hydroxide; water / ethanol / 20 °C View Scheme
参考文献
Nitta, Aiko; Fujii, Hideaki; Sakami, Satoshi; Satoh, Mikiya; Nakaki, Junko; Satoh, Shiho; Kumagai, Hiroki; Kawai, Hideki
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 23 p. 7036 - 7040
反应条件
potassium carbonate in ethanol T=20°C; 20 h;
参考文献
Dehmel, Florian; Ciossek, Thomas; Maier, Thomas; Weinbrenner, Steffen; Schmidt, Beate; Zoche, Martin; Beckers, Thomas
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 17 p. 4746 - 4752
反应条件
1: 2-bromo-4'-methoxy-acetophenone With 1,4-diaza-bicyclo[2.2.2]octane in water T=20°C; 2: With potassium carbonate in water T=20°C; 3: EtSCN in water Reflux;
参考文献
Kianmehr, Ebrahim; Mirza Agha, Mansoureh; Estiri, Hamid
Monatshefte fur Chemie, 2010 , vol. 141, # 4 p. 409 - 411
反应条件
AcrH2 in acetonitrile T=298°C; 19 h; Irradiation;
参考文献
Fukuzumi, Shunichi; Mochizuki, Seiji; Tanaka, Toshio
Journal of Physical Chemistry, 1990 , vol. 94, # 2 p. 722 - 726
反应条件
sodium formate; N-hexadecyl-N,N,N-trimethylammonium bromide; sodium lauryl sulfate; (R,R)-TsDPEN; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in water T=28°C; 1 h;
参考文献
Wang, Fei; Liu, Hui; Cun, Linfeng; Zhu, Jin; Deng, Jingen; Jiang, Yaozhong
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9424 - 9429
反应条件
C31H33ClN2O8RhS3(2-)*2Na(1+); sodium formate in water T=40°C; 1 h; Inert atmosphere; enantioselective reaction;
参考文献
RSC Advances, , vol. 3, # 6 p. 1825 - 1834
反应条件
di-n-butyltin dihydride 1 h; Ambient temperaturep-dinitrobenzene (DNB) as additive; Product distribution;
参考文献
Shibata, Ikuya; Nakamura, Kenji; Baba, Akio; Matsuda, Haruo
Tetrahedron Letters, 1990 , vol. 31, # 44 p. 6381 - 6384
反应条件
AcrD2; perchloric acid in acetonitrile T=61.9°C; primary kinetic isotope effect; Product distributionMechanism;
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1497 - 1499
反应条件
perchloric acid; 10-methyl-9,10-dihydroacridine in acetonitrile-D3 T=61.9°C; 4 h; Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 9 p. 3049 - 3051
反应条件
potassium iodide in acetone T=20°C; 2.25 h;
参考文献
Li, Hong Sheng; Li, Yi Qun
Chinese Chemical Letters, 2010 , vol. 21, # 8 p. 931 - 934
