alpha-溴-4-甲氧基苯乙酮合成路线 （共 261 条）
反应条件
1: in acetone
1 h; Heating;
2: With potassium carbonate
5 h;
参考文献
Chai, Wenying; Breitenbucher, J. Guy; Kwok, Annette; Li, Xiaobing; Wong, Victoria; Carruthers, Nicholas I.; Lovenberg, Timothy W.; Mazur, Curt; Wilson, Sandy J.; Axe, Frank U.; Jones, Todd K.
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 10 p. 1767 - 1770
反应条件
1: acetone / 4 h / Heating
2: 22 g / K2CO3 / H2O / 8 h / 80 °C
View Scheme
参考文献
Anitha; Rajan
Journal of the Indian Chemical Society, 1989 , vol. 66, # 7 p. 460 - 462
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
T=20°C; Rap-Stoermer reaction; 0.166667 h;
参考文献
Meshram; Reddy, B. Chennakesava; Prasad; Goud, P. Ramesh; Kumar, G. Santosh; Kumar, R. Naveen
Synthetic Communications, 2012 , vol. 42, # 11 p. 1669 - 1676
反应条件
potassium carbonate in 1,2-dichloro-ethane
4.5 h; RefluxInert atmosphere;
参考文献
Aljaar, Nayyef; Malakar, Chandi C.; Conrad, Ju Rgen; Frey, Wolfgang; Beifuss, Uwe
Journal of Organic Chemistry, 2013 , vol. 78, # 1 p. 154 - 166
参考文献
Bahner et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 1472
反应条件
bioglycerol-based sulfonic acid functionalized carbon in acetonitrile
2 h; RefluxGreen chemistry;
参考文献
Yang, Xiaojuan; Wu, Liqiang
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 10 p. 1327 - 1333
反应条件
in diethyl ether
T=20°C; Inert atmosphere;
参考文献
Sabatini, Stefano; Kaatz, Glenn W.; Rossolini, Gian Maria; Brandini, David; Fravolini, Arnaldo
Journal of Medicinal Chemistry, 2008 , vol. 51, # 14 p. 4321 - 4330
反应条件
1: N,N-dimethylaniline / 170 °C
2: POCl3 / 80 °C
View Scheme
参考文献
Nyerges, Miklos; Pinter, Aron; Viranyi, Andrea; Bitter, Istvan; Toke, Laszlo
Tetrahedron Letters, 2005 , vol. 46, # 3 p. 377 - 380
反应条件
1: 53 percent / aq. KOH / various solvent(s) / Ambient temperature
2: 52 percent / acetic acid / 0.67 h / Heating
View Scheme
参考文献
Shvedov, V. I.; Safonova, O. A.; Bulanova, T. I.; Il'ina, A. S.; Shvarts, G. Ya.; et al.
Pharmaceutical Chemistry Journal, 1980 , vol. 14, # 11 p. 794 - 798
Khimiko-Farmatsevticheskii Zhurnal, 1980 , vol. 14, # 11 p. 67 - 71
参考文献
Beyer,H.; Pommerening,K.
Chemische Berichte, 1966 , vol. 99, p. 2931 - 2936
