2,4,6-三甲基苯溴化镁合成路线 (共 186 条)
反应条件
boron trifluoride diethyl etherate
参考文献
Chu; Weismann
Journal of the American Chemical Society, 1956 , vol. 78, p. 23,24
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Brown; Dodson
Journal of the American Chemical Society, 1957 , vol. 79, p. 2302,2304
反应条件
phosphorus trichoride in diethyl ether
参考文献
Chemical Communications, , # 6 p. 583 - 584
反应条件
phosphorus trichoride in tetrahydrofuran T=-78 - 20°C; 12 h; Inert atmosphereSchlenk technique;
参考文献
Inorganic Chemistry, , vol. 52, # 11 p. 6694 - 6704
反应条件
phosphorus trichoride in tetrahydrofuran T=-50°C; further reagent: PBr3; Yield given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 116, # 5 p. 1947 - 1954
反应条件
hydrolysis with dild. HCl;;
参考文献
Gmelin Handbook: B: B-Verb.13, 4.7.2.7, page 226 - 237
反应条件
diethyl ether T=-78°C; und anschliessend mit wss.HCl;
参考文献
Hawthorne
Journal of Organic Chemistry, 1958 , vol. 23, p. 1579
参考文献
Lapkin,I.I.; Karavanov,N.A.
Zhurnal Organicheskoi Khimii, 1966 , vol. 2, p. 17 - 19,14 - 15
参考文献
Kohler, Baltzly
Journal of the American Chemical Society, 1932 , vol. 54, p. 4015,4022
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Nauta; Wuis
Recueil des Travaux Chimiques des Pays-Bas, 1937 , vol. 56, p. 535,540
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Coops et al.
Recueil des Travaux Chimiques des Pays-Bas, 1940 , vol. 59, p. 1109,1111
反应条件
diethyl ether; benzene
参考文献
Fuson; Corse; Rabjohn
Journal of the American Chemical Society, 1941 , vol. 63, p. 2852
参考文献
Lapkin
Zhurnal Obshchei Khimii, 1946 , vol. 16, p. 729,732,733
Chem. Zentralbl., 1947 , vol. 118, p. 1218