1,3-二甲基-2-叠氮基苯合成路线 (共 7 条)
反应条件
4-(N,N-dimethlyamino)pyridine; ADMP in dichloromethane T=50°C; 3.5 h; Inert atmosphere;
参考文献
Kitamura, Mitsuru; Yano, Masakazu; Tashiro, Norifumi; Miyagawa, Satoshi; Sando, Mitsuyoshi; Okauchi, Tatsuo
European Journal of Organic Chemistry, 2011 , # 3 p. 458 - 462
反应条件
sodium hydrogen telluride in diethyl ether; ethanol 0.25 h; Ambient temperature;
参考文献
Suzuki, Hitomi; Takaoka, Koji
Chemistry Letters, 1984 , p. 1733 - 1736
反应条件
trifluorormethanesulfonic acid; trifluoroacetic acid T=25°C; 4 h;
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 3156 - 3188
反应条件
T=-261.2°C; 2 h; Irradiation;
参考文献
Dunkin, Ian R.; Donnelly, Thomas; Lockhart, Thomas S.
Tetrahedron Letters, 1985 , vol. 26, # 3 p. 359 - 362
反应条件
carbon monoxide T=-243.2°C; 1 h; Irradiationphotolysis by var. wavelengths investigated: var. times and temperaturesin N2 and CO matrices.; Product distribution;
参考文献
Dunkin, Ian R.; Donnelly, Thomas; Lockhart, Thomas S.
Tetrahedron Letters, 1985 , vol. 26, # 3 p. 359 - 362
反应条件
1: 100 percent / sodium hydrogentelluide (NaTeH) / ethanol; diethyl ether / 0.25 h / Ambient temperature
2: tosylation
View Scheme
参考文献
Suzuki, Hitomi; Takaoka, Koji
Chemistry Letters, 1984 , p. 1733 - 1736
反应条件
aluminum tri-bromide
1 h; Heating;
参考文献
Takeuchi, Hiroshi; Shiobara, Yukihiko; Kawamoto, Hideyuki; Koyama, Kikuhiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 2 p. 321 - 327