Alpha-对甲苯磺酰基(4-甲氧基-苄基)异腈合成路线 (共 4 条)
反应条件
triethylamine; trichlorophosphate in tetrahydrofuran T=0°C; Yield given;
参考文献
Sisko, Joseph; Mellinger, Mark; Sheldrake, Peter W.; Baine, Neil H.
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8113 - 8116
反应条件
1: 92 percent / TMSCl / toluene; acetonitrile / 5 h / 50 °C 2: POCl3, Et3N / tetrahydrofuran / 0 °C View Scheme
参考文献
Sisko, Joseph; Mellinger, Mark; Sheldrake, Peter W.; Baine, Neil H.
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8113 - 8116
反应条件
1: 92 percent / TMSCl / toluene; acetonitrile / 5 h / 50 °C 2: POCl3, Et3N / tetrahydrofuran / 0 °C View Scheme
参考文献
Sisko, Joseph; Mellinger, Mark; Sheldrake, Peter W.; Baine, Neil H.
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8113 - 8116
反应条件
1: With chloro-trimethyl-silane 2: With triethylamine; trichlorophosphate
参考文献
Plante, Jeffrey P.; Glass, Timothy E.
Organic Letters, 2006 , vol. 8, # 10 p. 2163 - 2166