1,2-苯并异噻唑-3-酮合成路线 （共 63 条）
反应条件
pyridine; diphenyl phosphoryl azide; triethylamine T=20°C; Cyclization; 6 h;
参考文献
Chiyoda; Iida; Takatori; Kajiwara
Synlett, 2000 , # 10 p. 1427 - 1428
反应条件
sulfuryl dichloride in water
参考文献
Sumitomo Seika Chemicals Co., Ltd.
Patent: US5633384 A1, 1997 ;
反应条件
tetrachloromethane; chlorine Eintragen des Reaktionsprodukts in Ammoniak;
参考文献
Kamigata, Nobumasa; Hashimoto, Satoshi; Kobayashi, Michio; Nakanishi, Hiroshi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 11 p. 3131 - 3136
反应条件
sodium hydroxide; sulfuryl dichloride; tetrabutylammomium bromide; sodium in water
参考文献
Sumitomo Seika Chemicals Co., Ltd.
Patent: US5633384 A1, 1997 ;
反应条件
sodium methylate in dichloromethane T=20°C; Cyclization; alkoxylation; 2.5 h;
参考文献
Shimizu, Masao; Kikumoto, Hisashi; Konakahara, Takeo; Gama, Yasuo; Shibuya, Isao
Heterocycles, 1999 , vol. 51, # 12 p. 3005 - 3012
反应条件
1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; 1,10-phenanthroline; tetra-(n-butyl)ammonium iodide in water T=20 - 140°C; 48.5 h; Inert atmosphere;
参考文献
Wang, Fei; Chen, Chao; Deng, Geng; Xi, Chanjuan
Journal of Organic Chemistry, 2012 , vol. 77, # 8 p. 4148 - 4151
反应条件
hydroxylamine hydrochloride; sodium hydroxide in methanol; water T=20°C;
参考文献
Griffith, Darren M.; Haughey, Aisleen; Chahal, Sunisha; Mueller-Bunz, Helge; Marmion, Celine J.
Inorganica Chimica Acta, 2010 , vol. 363, # 10 p. 2333 - 2337
反应条件
ammonia in dichloromethane 1 h; Ambient temperature;
参考文献
Kim, Woongki; Dannaldson, Jeffrey; Gates, Kent S.
Tetrahedron Letters, 1996 , vol. 37, # 30 p. 5337 - 5340
反应条件
1.1: aq. NaOH / 3 h / 25 °C 2.1: NaOMe; CH3CONH2 / toluene / 2 h / 80 °C 2.2: aq. H2O2 / 50 - 55 °C 2.3: 90 percent / aq. HCl / 25 °C View Scheme
参考文献
Miura, Yozo
Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2850 - 2852
参考文献
Sumitomo Seika Chemicals Co., Ltd.; Sumitomo Chemical Co., Ltd.
Patent: US5508416 A1, 1996 ;
