oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane
T=-78 - 20°C;
参考文献
Carroll, F. Ivy; Melvin, Matt S.; Nuckols, Michel C.; Mascarella, S. Wayne; Navarro, Hernan A.; Thomas, James B.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 5 p. 1781 - 1791
1: With phenyl silane; 4-methylmorpholine N-oxide; molybdenum hexacarbonate in tetrahydrofuran
T=70°C; Inert atmosphere;
2: With water in tetrahydrofuran
T=20°C; Inert atmosphere;
参考文献
Maki, Brooks E.; Scheldt, Karl A.
Organic Letters, 2008 , vol. 10, # 19 p. 4331 - 4334
Carroll, F. Ivy; Melvin, Matt S.; Nuckols, Michel C.; Mascarella, S. Wayne; Navarro, Hernan A.; Thomas, James B.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 5 p. 1781 - 1791