(1H-吲哚-3-基磺酰基)盐酸乙脒碘化氢合成路线 （共 8 条）
反应条件
iodine; potassium iodide in methanol; water Ambient temperature;
参考文献
Nagarajan, K.; Arya, V. P.; Parthasarathy, T. N.; Shenoy, S. J.; Shah, R. K.; Kulkarni, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 672 - 679
反应条件
1: With sodium hydroxide; water 0.25 h; Inert atmosphereReflux; 2: With hydrogenchloride in water
参考文献
Csomos, Peter; Fodor, Lajos; Bernath, Gabor; Csampai, Antal; Sohar, Pal
Tetrahedron, 2009 , vol. 65, # 7 p. 1475 - 1480
反应条件
sodium hydroxide T=80°C; 0.5 h;
参考文献
Nagarajan, K.; Arya, V. P.; Parthasarathy, T. N.; Shenoy, S. J.; Shah, R. K.; Kulkarni, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 672 - 679
反应条件
1: 8 g / 10percent aq. NaOH / 0.5 h / 80 °C
2: 4.7 g / Triethyl amine / 8 h / Heating
View Scheme
参考文献
Nagarajan, K.; Arya, V. P.; Parthasarathy, T. N.; Shenoy, S. J.; Shah, R. K.; Kulkarni, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 672 - 679
反应条件
sodium hydroxide
T=80°C; 0.5 h;
参考文献
Nagarajan, K.; Arya, V. P.; Parthasarathy, T. N.; Shenoy, S. J.; Shah, R. K.; Kulkarni, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 672 - 679
反应条件
1: 8 g / 10percent aq. NaOH / 0.5 h / 80 °C
2: aq. NaOH
View Scheme
参考文献
Nagarajan, K.; Arya, V. P.; Parthasarathy, T. N.; Shenoy, S. J.; Shah, R. K.; Kulkarni, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 672 - 679
反应条件
1: With NH2NH2•xH2O; sodium hydroxide in ethanol; water
2 h; HeatingInert atmosphere;
2: With hydrogenchloride in water
T=5°C; pH=1; 12 h;
参考文献
Mirskova; Levkovskaya; Kolesnikova; Perminova; Rudyakova; Adamovich
Russian Chemical Bulletin, 2010 , vol. 59, # 12 p. 2236 - 2246
反应条件
1: 8 g / 10percent aq. NaOH / 0.5 h / 80 °C
2: anhydrous potassium carbonate / acetone / 8 h / Heating
View Scheme
参考文献
Nagarajan, K.; Arya, V. P.; Parthasarathy, T. N.; Shenoy, S. J.; Shah, R. K.; Kulkarni, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 672 - 679
