4,4'-偶氮双(4-氰基戊酸)合成路线 （共 8 条）
反应条件
sulfuric acid; water; hydrazine Behandeln des Reaktionsgemisches mit Brom; optically inactive stereoisomer(ic) of mp: 111 degree;
参考文献
Haines; Waters
Journal of the Chemical Society, 1955 , p. 4256,4259
反应条件
1: dithiobenzoic acid sodium salt With iodine in water 1 h; 2: V-501 in ethyl acetate 18 h;
参考文献
Kim, Hee-Jung; Kim, Dong-Ryul
Patent: US2004/138492 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
in ethyl acetate T=85°C; 12 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 38 p. 10656 - 10658
反应条件
pyrrol-N-thiocarbonyl disulfides in ethyl acetate 20 h;
参考文献
US2004/138492 A1, ;
Page 4 ;
反应条件
in methanol T=80°C; 3 h;
参考文献
Chemical Communications, , # 19 p. 2230 - 2232
反应条件
1: m-dithiobenzoic acid With iodine; dimethyl sulfoxide in ethyl acetate 10 h; 2: V-501 in ethyl acetate 18 h; Heating;
参考文献
Macromolecules, , vol. 38, # 16 p. 6841 - 6848
反应条件
in ethyl acetate T=20°C; 28 h; Reflux;
参考文献
Chemistry - An Asian Journal, , vol. 9, # 1 p. 199 - 205
反应条件
in ethyl acetate
16 h; Heating / reflux;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2005/113493 A1, 2005 ;
Location in patent: Page/Page column 3; 4-5 ;
