N-(2-氯乙基)苯甲酰胺合成路线 （共 47 条）
反应条件
n-butyllithium; naphthalenyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 8 h, 2.) -78 deg C, 1 h; -78 deg C to r.t., overnight;
参考文献
Journal of Organic Chemistry, , vol. 58, # 22 p. 5976 - 5980
反应条件
n-butyllithium; naphthalenyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 8 h, 2.) -78 deg C, 1 h; -78 deg C to r.t., overnight;
参考文献
Journal of Organic Chemistry, , vol. 58, # 22 p. 5976 - 5980
反应条件
1: 61 percent / NaI, CH3I, N-methyl-2-pyrrolidinone / 96 h / 70 °C 2: 80 percent / butyllithium / tetrahydrofuran; hexane / 1.) -78 deg C, 30 min, 2.) -78 to 20 deg C, overnight View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 22 p. 5976 - 5980
反应条件
n-butyllithium; naphthalenyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 8 h, 2.) -78 deg C, 1 h; -78 deg C to r.t., overnight;
参考文献
Barluenga, Jose; Montserrat, Javier M.; Florez, Josefa
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 5976 - 5980
反应条件
2: 1N HCl View Scheme
参考文献
Barluenga, Jose; Montserrat, Javier M.; Florez, Josefa
Tetrahedron Letters, 1992 , vol. 33, # 41 p. 6183 - 6186
反应条件
n-butyllithium; naphthalenyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 8 h, 2.) -78 deg C, 1 h; -78 deg C to r.t., overnight;
参考文献
Barluenga, Jose; Montserrat, Javier M.; Florez, Josefa
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 5976 - 5980
反应条件
1: n-buthyl-lithium, lithium naphthalenide / tetrahydrofuran; diethyl ether / 4 h / -78 °C 2: H2O / -78 - 20 °C View Scheme
参考文献
Tetrahedron, , vol. 45, # 7 p. 2183 - 2192
反应条件
n-butyllithium; naphthalenyllithium 1.) THF, ether, -78 deg C, 20 min 2.) THF, 5 h, -78 deg C; 3.) 20 deg C; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 29, # 23 p. 2859 - 2860
反应条件
1: phosphorus (V)-chloride / 100 °C View Scheme
参考文献
Partridge; Turner
Journal of the Chemical Society, 1949 , p. 1308
反应条件
phosphorus pentachloride
参考文献
Partridge; Turner
Journal of the Chemical Society, 1949 , p. 1308
