N-(2-氯乙基)苯甲酰胺合成路线 （共 47 条）
反应条件
n-butyllithium; naphthalenyllithium; ortho-dibromobenzene in tetrahydrofuran; hexane 1.) -78 deg C, 8 h, 2.) -78 deg C to r.t.;
参考文献
Barluenga, Jose; Montserrat, Javier M.; Florez, Josefa
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 5976 - 5980
反应条件
aluminium trichloride
参考文献
Rodionow et al.
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 734,739; engl. Ausg. S. 809, 813
参考文献
Fry
Journal of Organic Chemistry, 1949 , vol. 14, p. 887,891
参考文献
Fry
Journal of Organic Chemistry, 1949 , vol. 14, p. 887,891
反应条件
n-butyllithium; naphthalenyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 8 h, 2.) -78 deg C, 1 h; -78 deg C to r.t., overnight;
参考文献
Barluenga, Jose; Montserrat, Javier M.; Florez, Josefa
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 5976 - 5980
反应条件
n-butyllithium; oxygen; naphthalenyllithium
1.) THF, ether, -78 deg C, 20 min 2.) THF, 5 h, -78 deg C; 3.) 20 deg C; Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Foubelo, Francisco; Fananas, Francisco J.; Yus, Miguel
Tetrahedron, 1989 , vol. 45, # 7 p. 2183 - 2192
反应条件
1: With Lawesson's reagent in toluene
1 h; Heating;
2: With triethylamine in toluene
T=20°C;
参考文献
Kodama, Yasuhiro; Ori, Mayuko; Nishio, Takehiko
Helvetica Chimica Acta, 2005 , vol. 88, # 2 p. 187 - 193
反应条件
1: AgBF4 / acetonitrile / 16 h / Ambient temperature
View Scheme
参考文献
Tomalia,D.A.; Paige,J.N.
Journal of Organic Chemistry, 1973 , vol. 38, # 3 p. 422 - 430
反应条件
sodium azide in N,N-dimethyl-formamide
参考文献
Gusar',N.I. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1979 , vol. 49, # 8 p. 1782 - 1787,1565 - 1569
反应条件
1: NaN3 / dimethylformamide
2: benzene / Ambient temperature
3: benzene / Heating
View Scheme
参考文献
Gusar',N.I. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1979 , vol. 49, # 8 p. 1782 - 1787,1565 - 1569
