4-(2-甲氧基苯基)苯胺合成路线 （共 11 条）
反应条件
ammonium formate; palladium on activated charcoal in methanol T=20°C; 3 h;
参考文献
Takahashi, Hidenori; Bekkali, Younes; Capolino, Alison J.; Gilmore, Thomas; Goldrick, Susan E.; Nelson, Richard M.; Terenzio, Donna; Wang, Ji; Zuvela-Jelaska, Ljiljana; Proudfoot, John; Nabozny, Gerald; Thomson, David
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 6 p. 1549 - 1552
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; water T=20°C; 12 h;
参考文献
Pena-Lopez, Miguel; Sarandeses, Luis A.; Perez Sestelo, Jose
European Journal of Organic Chemistry, 2013 , # 13 p. 2545 - 2554
反应条件
K3PO4*7H2O; palladium diacetate in water; N,N-dimethyl-formamide T=80°C; Suzuki Coupling; 2 h;
参考文献
Liu, Chun; Song, Xiaoxiao; Ni, Qijian; Qiu, Jieshan
ARKIVOC (Gainesville, FL, United States), 2012 , vol. 2012, # 9 p. 62 - 75,14
反应条件
{C6H3[NHP(piperidinyl)2]2Pd(Cl)}; potassium carbonate in 1,4-dioxane; water; butan-1-ol T=100°C; Suzuki-Miyaura reaction; 4 h;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 6 p. 1075 - 1080
反应条件
caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Suzuki cross-coupling reaction; Heating;
参考文献
Slegt, Micha; Overkleeft, Hermen S.; Lodder, Gerrit
European Journal of Organic Chemistry, 2007 , # 32 p. 5364 - 5375
反应条件
1: 70 percent / Pd(PPh3)2Cl2 / dimethylformamide / 0.25 h / 160 °C / microwave irradiation 2: 99 percent / HCOONH4 / Pd/C / methanol / 3 h / 20 °C View Scheme
参考文献
Takahashi, Hidenori; Bekkali, Younes; Capolino, Alison J.; Gilmore, Thomas; Goldrick, Susan E.; Nelson, Richard M.; Terenzio, Donna; Wang, Ji; Zuvela-Jelaska, Ljiljana; Proudfoot, John; Nabozny, Gerald; Thomson, David
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 6 p. 1549 - 1552
反应条件
1: 70 percent / Pd(PPh3)2Cl2 / dimethylformamide / 0.25 h / 160 °C / microwave irradiation 2: 99 percent / HCOONH4 / Pd/C / methanol / 3 h / 20 °C View Scheme
参考文献
Takahashi, Hidenori; Bekkali, Younes; Capolino, Alison J.; Gilmore, Thomas; Goldrick, Susan E.; Nelson, Richard M.; Terenzio, Donna; Wang, Ji; Zuvela-Jelaska, Ljiljana; Proudfoot, John; Nabozny, Gerald; Thomson, David
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 6 p. 1549 - 1552
反应条件
PPA; trifluoroacetic acid T=50°C; Substitution; decomposition; trifluoroacetylation; 3 h; Further byproducts. Title compound not separated from byproducts.;
参考文献
Takeuchi, Hiroshi; Taniguchi, Tomohito; Ueda, Takahiro
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 2 p. 295 - 300
反应条件
1: aqueous NaOH / 60 °C 2: aqueous ethanol; iron; acetic acid View Scheme
参考文献
Harley-Mason; Mann
Journal of the Chemical Society, 1940 , p. 1379,1381
反应条件
in acetonitrile T=2°C; Photolysis; Product distribution;
参考文献
Slegt, Micha; Overkleeft, Hermen S.; Lodder, Gerrit
European Journal of Organic Chemistry, 2007 , # 32 p. 5364 - 5375
