2,5-双(三氟甲基)-3,6-二氧杂十一氟代壬酰氟合成路线 （共 33 条）
反应条件
in diethyl ether at 0°C after 3.5 h only 25 percent of C6F5MgBr reacted, then allowing the mixt. to warm to 20°C and stirring for another 48 h, hydrolysis;
参考文献
Journal of Fluorine Chemistry, , vol. 13, p. 337,339, 340, 344, 348
反应条件
water 1 h; Ambient temperature;
参考文献
Tatarinova, E. L.; Zachinyaev, Ya.V.; Popova, L.M.; Ryabinin, N.A.; Ginak, A.I.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 7.2 p. 1677 - 1678,1379 - 1380
反应条件
1: 86.3 percent / Na2CO3; MgSO4; silica gel / diethyl ether / 20 °C 2: 81.1 percent / NaBH4 / diethyl ether; methanol / 12 h / Heating View Scheme
参考文献
Paleta, Oldrich; Palecek, Jiri; Michalek, Jiri
Journal of Fluorine Chemistry, 2002 , vol. 114, # 1 p. 51 - 53
反应条件
sodium carbonate in diethylene glycol dimethyl ether T=20°C; Elimination; 52 h;
参考文献
Journal of Fluorine Chemistry, , vol. 106, # 1 p. 13 - 24
反应条件
potassium fluoride in acetonitrile T=70°C; 4 h; Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
potassium fluoride in acetonitrile T=75°C; 15 h;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
potassium fluoride in acetonitrile T=75°C; 20 h; Further byproducts given. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
potassium fluoride in acetonitrile T=70°C; 16 h;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
cesium fluoride in diethyl ether T=0°C; 3 h; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 69, # 1 p. 61 - 66
反应条件
potassium fluoride in acetonitrile also with CsF; also with Br2 and further substrates; Product distributionMechanism;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
