1,3-二(苯基)-1-(苯基氨基甲酰)脲合成路线 （共 27 条）
反应条件
3, 4-dimethoxybenzaldehyde oxime; triethylamine in benzene
参考文献
Wiegrebe,W. et al.
Helvetica Chimica Acta, 1976 , vol. 59, p. 949 - 962
参考文献
Habib, Nargues S.; Rieker, Anton
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1984 , vol. 39, # 11 p. 1593 - 1597
反应条件
in hexane
under N2; dry hexane; refluxed for 2 h; orange soln. became burgundy red; whitish ppt. sepd.; dissolved in warm CH2Cl2; slow cooling at 0°C; identified as biuret by IR, (1)H NMR, MS; red supernatant liquid was syringed off; TLC showed one band; soln. was concd. and cooled to -20°C; elem. anal.;
参考文献
Crocq, Veronique; Daran, Jean-Claude; Jeannin, Yves
Journal of Organometallic Chemistry, 1989 , vol. 373, p. 85 - 98
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
16 h; Reflux;
参考文献
Mrkvicka, Vladimir; Lycka, Antonin; Vicha, Robert; Klasek, Antonin
Helvetica Chimica Acta, 2011 , vol. 94, # 1 p. 78 - 91
反应条件
1.1: ethylene dibromide / tetrahydrofuran / |Inert atmosphere; |Heating
1.2: 0.25 h / 20 °C / |Inert atmosphere
1.3: 20 °C / |Inert atmosphere
2.1: tetrahydrofuran / 8 h / -45 °C / |Inert atmosphere
2.2: |Inert atmosphere
View Scheme
参考文献
Yang, Haoran; Huang, Danfeng; Wang, Ke-Hu; Xu, Changming; Niu, Teng; Hu, Yulai
Tetrahedron, 2013 , vol. 69, # 12 p. 2588 - 2593
反应条件
carbon monoxide in 1,2-dichloro-benzene
byproducts: CO2; heating in o-dichlorobenzene under CO (20 bar) at 170°C;
参考文献
Leconte, P.; Metz, F.; Mortreux, A.; Osborn, J. A.; Paul, F.; et al.
Journal of the Chemical Society, Chemical Communications, 1990 , # 22 p. 1616 - 1617
反应条件
in pyridine
10 h; Heating;
参考文献
Youssef, Ahmed S.A.; Kandeel, Kamal A.; Fouli, Fouli A.; Abou-Elmagd, Wael S.I.
Heteroatom Chemistry, 2005 , vol. 16, # 1 p. 6 - 11
反应条件
in pyridine
10 h; Heating;
参考文献
Youssef, Ahmed S.A.; Kandeel, Kamal A.; Fouli, Fouli A.; Abou-Elmagd, Wael S.I.
Heteroatom Chemistry, 2005 , vol. 16, # 1 p. 6 - 11
参考文献
Kuehn; Hentschel
Chemische Berichte, 1888 , vol. 21, p. 504
参考文献
Baker; Holdsworth
Journal of the Chemical Society, 1945 , p. 724,731
