2,3-二氢-1H-茚-1-甲腈合成路线 （共 18 条）
反应条件
hydrogen; palladium on activated carbon in ethanol
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2004/55012 A1, 2004 ;
Location in patent: Page 53 ;
WO 2004/055012 A1
反应条件
phenyl silane; ethanediamino-N,N'-bis(salicylidene)-based cobalt catalyst in ethanol T=23°C; 1 h;
参考文献
Gaspar, Boris; Carreira, Erick M.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 24 p. 4519 - 4522
反应条件
potassium tert-butylate in ethylene glycol dimethyl ether; tert-butyl alcohol T=20°C; Condensation; 48 h;
参考文献
Dalko, Peter I.; Langlois, Yves
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8107 - 8117
反应条件
Ki in N,N-dimethyl-formamide
参考文献
Regents of the University of Minnesota
Patent: US5948807 A1, 1999 ;
US 5948807 A
反应条件
in N,N-dimethyl-formamide T=50°C; 6 h;
参考文献
Crombie, Leslie; Tuchinda, Patoomratana; Powell, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1477 - 1484
反应条件
in dimethyl sulfoxide T=140°C; 2 h; Inert atmosphere;
参考文献
Fuchibe, Kohei; Mayumi, Yuka; Zhao, Nan; Watanabe, Shumpei; Yokota, Misaki; Ichikawa, Junji
Angewandte Chemie - International Edition, 2013 , vol. 52, # 30 p. 7825 - 7828
Angew. Chem., 2013 , vol. 125, # 30 p. 7979 - 7982,4
反应条件
Na2S2O5; trichlorophosphate
参考文献
Ray; Lahiri
Journal of the Indian Chemical Society, 1990 , vol. 67, # 4 p. 324 - 326
反应条件
1: SOCl2, pyridine 2: aq. ethanol 3: K, NH3 View Scheme
参考文献
Bunnett,J.F.; Skorcz,J.A.
Journal of Organic Chemistry, 1962 , vol. 27, p. 3836 - 3843
反应条件
1: aq. ethanol 2: K, NH3 View Scheme
参考文献
Bunnett,J.F.; Skorcz,J.A.
Journal of Organic Chemistry, 1962 , vol. 27, p. 3836 - 3843
反应条件
1: LiAlH4 / diethyl ether 2: SOCl2, pyridine 3: aq. ethanol 4: K, NH3 View Scheme
参考文献
Bunnett,J.F.; Skorcz,J.A.
Journal of Organic Chemistry, 1962 , vol. 27, p. 3836 - 3843
