1-(4-溴苯基)-2-硫代脲合成路线 (共 15 条)
参考文献
Cymerman-Craig et al.
Org.Synth.Coll., 1963 , vol. Vol.IV, p. 700
反应条件
disulfur dichloride T=60°C;
参考文献
Helvetica Chimica Acta, , vol. 63, # 3 p. 682 - 692
反应条件
1: bromine / chloroform / 0 - 5 °C / Reflux
2: pyridine / 6 h / Reflux
View Scheme
参考文献
Sharma, Pratibha; Kumar, Ashok; Kumari, Prerna; Singh, Jitendra; Kaushik
Medicinal Chemistry Research, 2012 , vol. 21, # 7 p. 1136 - 1148
反应条件
copper(l) iodide; sodium hydroxide in dimethyl sulfoxide
T=90°C; 3 h;
参考文献
Sahoo, Santosh K.; Jamir, Latonglila; Guin, Srimanta; Patel, Bhisma K.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2538 - 2548
反应条件
1: in ethanol
T=30 - 35°C; Hantzsch reaction; 2.25 h; Sonication;
2: With ammonium hydroxide in ethanol
参考文献
Gupta, Ragini; Sharma, Deepti; Singh, Swaroop
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1321 - 1331