3,3-二甲基-2,3-二氢-1H-茚-1-酮合成路线 (共 47 条)
反应条件
AlCl3, aluminium chloride T=25 - 30°C; Nazarov Cyclization; 3.63333 h;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 365, p. 203 - 211
反应条件
AlCl3, aluminium chloride 5 h; Reflux;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 37 p. 9796 - 9800
Angew. Chem., , vol. 125, # 37 p. 9978 - 9982,5
反应条件
AlCl3, aluminium chloride T=25 - 30°C; Friedel-Crafts Acylation; 3.63333 h; Reflux;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 365, p. 203 - 211
反应条件
tert.-butylhydroperoxide; 4C12H25O4S(1-)*Fe2O(4+)*10H2O in water T=30°C; 50 h;
参考文献
Chemistry Letters, , vol. 37, # 10 p. 1042 - 1043
参考文献
Helvetica Chimica Acta, , vol. 53, p. 1323 - 1330
Yakugaku Zasshi, , vol. 76, p. 163,165, 166
Chem.Abstr., , p. 13850
反应条件
in diethyl ether 0.0833333 h; Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 111, # 8 p. 2883 - 2891
反应条件
sodium chloride in diethyl ether; ethyl acetate; benzene
参考文献
US5514690 A1, ;
US 5514690 A
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2; caesium carbonate; (R)-1,1'-bis(diphenylphosphino)-2,2'-binapthyl in anhydrous xylene T=23 - 120°C; 12.1667 h; Inert atmosphere;
参考文献
Synlett, , # 11 p. 1699 - 1703
反应条件
1: With tetrakis(triphenylphosphine) palladium(0); triphenylphosphine in N,N-dimethyl acetamide T=110°C; Heck-type 5-endo-trig cyclization; 9 h; 2: With phosphate buffer in N,N-dimethyl acetamide pH=7; Further stages.;
参考文献
Journal of Fluorine Chemistry, , vol. 127, # 4-5 SPEC. ISS. p. 489 - 504
反应条件
{1,3-bis[2,6-di(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}AuCl; AgNTf2 in 1,2-dichloro-ethane T=25°C; 0.4 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 12 p. 2939 - 2942