1-[2-氧-2-(2-吡啶基)乙基]碘化吡啶合成路线 （共 37 条）
反应条件
ammonium acetate in methanol
参考文献
Zhao, Long-Xuan; Kim, Tae Sung; Ahn, Soo-Hyun; Kim, Tae-Hyung; Kim, Eun-kyung; Cho, Won-Jea; Choi, Heesung; Lee, Chong-Soon; Kim, Jung-Ae; Jeong, Tae Cheon; Chang, Ching-jer; Lee, Eung-Seok
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 19 p. 2659 - 2662
反应条件
1: ammonium acetate / methanol / 20 h / |Reflux
2: palladium 10 on activated carbon; hydrazine hydrate / ethanol / 3 h / |Reflux
View Scheme
参考文献
Durrell, Alec C.; Li, Gonghu; Koepf, Matthieu; Young, Karin J.; Negre, Christian F.A.; Allen, Laura J.; McNamara, William R.; Song, Hee-Eun; Batista, Victor S.; Crabtree, Robert H.; Brudvig, Gary W.
Journal of Catalysis, 2014 , vol. 310, p. 37 - 44
反应条件
ammonium acetate in methanol
4 h; Heating;
参考文献
Chotalia, Rohit; Constable, Edwin C.; Hannon, Michael J.; Tocher, Derek A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , # 22 p. 3571 - 3580
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Chotalia, Rohit; Constable, Edwin C.; Neuburger, Markus; Smith, Diane R.; Zehnder, Margareta
Journal of the Chemical Society - Dalton Transactions, 1996 , # 22 p. 4207 - 4216
反应条件
ammonium acetate in methanol
Kroehnke reaction; 17 h; Heating;
参考文献
Constable, Edwin C.; Figgemeier, Egbert; Hougen, Inger Annette; Housecraft, Catherine E.; Neuburger, Markus; Schaffner, Silvia; Whall, Louise A.
Dalton Transactions, 2005 , # 7 p. 1168 - 1175
反应条件
ammonium acetate in acetic acid
Heating;
参考文献
Mutai, Toshiki; Cheon, Jin-Dong; Arita, Shinpei; Araki, Koji
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 7 p. 1045 - 1050
反应条件
1: methanol / Reflux
2: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane
View Scheme
参考文献
Das, Priyadip; Ghosh, Amrita; Kesharwani, Manoj K.; Ramu, Vadde; Ganguly, Bishwajit; Das, Amitava
European Journal of Inorganic Chemistry, 2011 , # 20 p. 3050 - 3058
反应条件
1: 99 percent / methacrolein; ammonium acetate; HCHO / 6 h / 75 °C
2: 48 percent / NBS; AIBN / CCl4 / 24 h / 45 °C
View Scheme
参考文献
Bos, Jeffrey; Fusetti, Fabrizia; Driessen, Arnold J. M.; Roelfes, Gerard
Angewandte Chemie - International Edition, 2012 , vol. 51, # 30 p. 7472 - 7475
反应条件
ammonium acetate in methanol
T=80°C; Kroehnke synthesis;
参考文献
Basnet, Arjun; Thapa, Pritam; Karki, Radha; Na, Younghwa; Jahng, Yurngdong; Jeong, Byeong-Seon; Jeong, Tae Cheon; Lee, Chong-Soon; Lee, Eung-Seok
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 13 p. 4351 - 4359
反应条件
in ethanol
3 h; Reflux;
参考文献
Constable, Edwin C.; Housecroft, Catherine E.; Kopecky, Peter; Martin, Colin J.; Wright, Iain A.; Zampese, Jennifer A.; Bolink, Henk J.; Pertegas, Antonio
Dalton Transactions, 2013 , vol. 42, # 22 p. 8086 - 8103
反应条件
ammonium acetate in methanol
参考文献
Zhao, Long-Xuan; Kim, Tae Sung; Ahn, Soo-Hyun; Kim, Tae-Hyung; Kim, Eun-kyung; Cho, Won-Jea; Choi, Heesung; Lee, Chong-Soon; Kim, Jung-Ae; Jeong, Tae Cheon; Chang, Ching-jer; Lee, Eung-Seok
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 19 p. 2659 - 2662
